3-(1,3-苯并噻唑-2-基氨基)-1-丙醇合成路线 (共 3 条)
反应条件
N-ethyl-N,N-diisopropylamine T=110°C; 13 h; Inert atmosphere;
参考文献
Woods, Philip A.; Morrill, Louis C.; Lebl, Tomas; Slawin, Alexandra M. Z.; Bragg, Ryan A.; Smith, Andrew D.
Organic Letters, 2010 , vol. 12, # 11 p. 2660 - 2663
反应条件
1: sodium hydrogencarbonate / acetone 2: tetrahydrofuran 3: tetrakis(triphenylphosphine) palladium(0); caesium carbonate / ethylene glycol dimethyl ether / 80 °C View Scheme
参考文献
Okamoto, Sentaro; Sakai, Yuzo; Watanabe, Saki; Nishi, Shohei; Yoneyama, Aya; Katsumata, Hitomi; Kosaki, Yu; Sato, Rumi; Shiratori, Megumi; Shibuno, Misuzu; Shishido, Tsukasa
Tetrahedron Letters, 2014 , vol. 55, # 11 p. 1909 - 1912
反应条件
1: tetrahydrofuran 2: tetrakis(triphenylphosphine) palladium(0); caesium carbonate / ethylene glycol dimethyl ether / 80 °C View Scheme
参考文献
Okamoto, Sentaro; Sakai, Yuzo; Watanabe, Saki; Nishi, Shohei; Yoneyama, Aya; Katsumata, Hitomi; Kosaki, Yu; Sato, Rumi; Shiratori, Megumi; Shibuno, Misuzu; Shishido, Tsukasa
Tetrahedron Letters, 2014 , vol. 55, # 11 p. 1909 - 1912