dimethylphenylsilane; C19H8O7Ru3 in 1,4-dioxane T=50°C; 3 h; Inert atmosphere;

tri-isobutyl aluminium in toluene T=20°C; Rearrangement; 2 h;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '11993489', constants.ctx, '0')">di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '4154566', constants.ctx, '0')">sodium carbonate</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '635760', constants.ctx, '0')">toluene</a> <br />T=100&deg;C;&nbsp;6&nbsp;h;&nbsp;&nbsp;Inert atmosphere;&nbsp;<br /> <br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: Et₃N<br />2: pyridine / tetrahydrofuran / -45 - 20 &deg;C<br /> <br /> &nbsp;