二乙基硫代氨基甲酸 S-苄酯合成路线 （共 12 条）
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=120°C; P=38000 Torr; 48 h;
参考文献
Nishiyama, Yutaka; Kawamatsu, Hiroaki; Sonoda, Noboru
Journal of Organic Chemistry, 2005 , vol. 70, # 7 p. 2551 - 2554
反应条件
1: carbon monoxide; diethylamine With sulfur in dimethyl sulfoxide T=20°C; P=760 Torr; 8 h; 2: benzyl chloride in dimethyl sulfoxide T=20°C; 1 h;
参考文献
Mizuno, Takumi; Iwai, Toshiyuki; Ishino, Yoshio
Tetrahedron, 2005 , vol. 61, # 38 p. 9157 - 9163
反应条件
1: N,N-diethyl-α,α,α-trichloroacetamide in tetrahydrofuran T=20°C; 0.25 h; 2: 4-chlorophenylmethanethiol T=20°C; 4 h; Heating / reflux;
参考文献
The United States of America as represented by the Secretary of the Navy
Patent: US6686494 B1, 2004 ;
Location in patent: Page column 9-10 ;
反应条件
sulfur; selenium in tetrahydrofuran 1.) 30 deg C; 2.) rt.;
参考文献
Mizuno, Takumi; Nishiguchi, Ikuzo; Sonoda, Noboru
Tetrahedron, 1994 , vol. 50, # 19 p. 5669 - 5680
反应条件
tetrakis(triphenylphosphine) palladium(0) in pyridine T=100°C; Carbonylation; P=14701.2 Torr; 20 h;
参考文献
Kuniyasu, Hitoshi; Hiraike, Hiroshi; Morita, Masaki; Tanaka, Aoi; Sugoh, Kunihiko; Kurosawa, Hideo
Journal of Organic Chemistry, 1999 , vol. 64, # 20 p. 7305 - 7308
反应条件
potassium hydroxide in acetone T=25 - 30°C; 24 h;
参考文献
D'Amico, John J.; Schafer, Tann
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 8, p. 301 - 304
反应条件
in water T=30°C; 0.166667 h; in ultrasonic field;
参考文献
Galiakhmetov, R. N.; Valitov, R. B.; Kurochkin, A. K.; Margulis, M. A.
Russian Journal of Physical Chemistry, 1986 , vol. 60, # 4 p. 614 - 615
Zhurnal Fizicheskoi Khimii, 1986 , vol. 60, p. 1024 - 1025
反应条件
sodium hydroxide 1.) from 0 deg C to 20 deg C, 4 h, 2.) 25-30 deg C, 18 h;
参考文献
D'Amico, John J.; Schafer, Tann
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 8, p. 301 - 304
反应条件
in acetone 1.) 6 h, reflux, 2.) 18 h, 25-30 deg C;
参考文献
D'Amico, John J.; Schafer, Tann
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 8, p. 301 - 304
反应条件
1: 45 percent / MCPBA, NaHCO3 / CH2Cl2 / 4 h / 0 °C 2: 1 h / 20 °C View Scheme
参考文献
Chevrie, David; Metzner, Patrick
Tetrahedron Letters, 1998 , vol. 39, # 49 p. 8983 - 8986
