2-二乙基膦酰基-2-氟乙酸合成路线 （共 17 条）
反应条件
n-butyllithium in tetrahydrofuran; hexane 1.) -78 deg C, 1 h; 2.) 15 h room temperature;
参考文献
Coutrot, Ph.; Grison, C.; Sauvetre, R.
Journal of Organometallic Chemistry, 1987 , vol. 332, p. 1 - 8
反应条件
1: SOCl2 / CH2Cl2 2: 20 percent / 3 h / -78 - -45 °C View Scheme
参考文献
Coutrot, Ph.; Grison, C.
Tetrahedron Letters, 1988 , vol. 29, # 22 p. 2655 - 2658
反应条件
1: SOCl2 / CH2Cl2 2: 10 percent / 3 h / -78 - -45 °C View Scheme
参考文献
Coutrot, Ph.; Grison, C.
Tetrahedron Letters, 1988 , vol. 29, # 22 p. 2655 - 2658
反应条件
n-butyllithium in tetrahydrofuran; hexane 1.) -78 deg C, 3 h; 2.) 15 h room temperature; Yield given. Title compound not separated from byproducts;
参考文献
Journal of Organometallic Chemistry, , vol. 332, p. 1 - 8
反应条件
n-butyllithium in tetrahydrofuran; hexane
1.) -78 deg C, 1 h; 2.) 15 h room temperature;
参考文献
Coutrot, Ph.; Grison, C.; Sauvetre, R.
Journal of Organometallic Chemistry, 1987 , vol. 332, p. 1 - 8
反应条件
iso-propylmagnesium bromide in tetrahydrofuran
Horner-Wadsworth-Emmons reaction; 1 h; Heating;
参考文献
Sano, Shigeki; Teranishi, Rie; Nagao, Yoshimitsu
Tetrahedron Letters, 2002 , vol. 43, # 50 p. 9183 - 9186
反应条件
sulfuric acid in various solvent(s)
24 h;
参考文献
Massoudi, Hosseine H.; Cantacuzene, Daniele; Wakselman, Claude; Bouthier de la Tour, Claire
Synthesis, 1983 , # 12 p. 1010 - 1012
