2-溴-1-(4-叔丁基苯基)-乙酮合成路线 (共 10 条)
反应条件
2-(dicyclohexylphosphino)-2',4',6'-triisopropylbiphenyl Au bis(trifluoromethylsulfonyl)imide; water in 1,2-dichloro-ethane T=20°C; 14 h;
参考文献
Chen, Zheng-Wang; Ye, Dong-Nai; Ye, Min; Zhou, Zhong-Gao; Li, Shen-Huan; Liu, Liang-Xian
Tetrahedron Letters, 2014 , vol. 55, # 7 p. 1373 - 1375
反应条件
Sodium bromate; sulfuric acid; sodium bromide in 1,4-dioxane; water T=20°C; 6 h;
参考文献
Tetrahedron Letters, , vol. 50, # 21 p. 2529 - 2532
反应条件
hydrogen bromide; oxygen in water; ethyl acetate 7 h; Irradiation;
参考文献
Nobuta, Tomoya; Hirashima, Shin-Ichi; Tada, Norihiro; Miura, Tsuyoshi; Itoh, Akichika
Synlett, 2010 , # 15 p. 2335 - 2339
反应条件
Oxonereg;; potassium bromide in dichloromethane; water T=20°C; 24 h; visible light irradiation;
参考文献
Organic Letters, , vol. 14, # 9 p. 2414 - 2417
反应条件
dihydrogen peroxide in 1,4-dioxane; water T=25°C; 9 h;
参考文献
Synthetic Communications, , vol. 40, # 21 p. 3233 - 3239
反应条件
1: N-bromosuccinmide; silver nitrate / acetone / 20 °C 2: water; 2-(dicyclohexylphosphino)-2',4',6'-triisopropylbiphenyl Au bis(trifluoromethylsulfonyl)imide / 1,2-dichloro-ethane / 14 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 78, # 18 p. 9190 - 9195
反应条件
1: manganese(IV) oxide / chloroform / 1 h / 65 °C 2: pyrrolidone trihydrobromide / tetrahydrofuran / 0.5 h / 60 °C View Scheme
反应条件
1: diethyl ether / 0.5 h / |Cooling with ice 2: manganese(IV) oxide / chloroform / 1 h / 65 °C 3: pyrrolidone trihydrobromide / tetrahydrofuran / 0.5 h / 60 °C View Scheme
参考文献
Bahner et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 3499
参考文献
Bahner et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 4198