1-甲基-2-甲酰苯并咪唑合成路线 (共 16 条)
反应条件
hydrogenchloride 1 h; Yield given. Yields of byproduct given;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 23, # 2 p. 284 - 287
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 23, # 2 p. 339 - 342
反应条件
1: aqueous methanol. NaOH 2: SeO2; toluene View Scheme
参考文献
Bulletin de la Societe Chimique de France, , p. 343,347
Rev. textile-Tiba, , vol. 57, p. 164,166
反应条件
1: 88 percent / diisobutylaluminium hydride / hexane; tetrahydrofuran / 1 h / 0 °C 2: 255 mg / SOCl2 / CH2Cl2 / 3 h View Scheme
参考文献
RECORDATI IRELAND LIMITED; LEONARDI, Amedeo; MOTTA, Gianni; RIVA, Carlo; GUARNERI, Luciano; GRAZIANI, Davide; MARINONI, Fabio; BETTINELLI, Ilaria
Patent: WO2011/29633 A1, 2011 ;
WO 2011/029633 A1
反应条件
diisobutylaluminium hydride in tetrahydrofuran; hexane T=0°C; 1 h;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 14, # 19 p. 6695 - 6712
反应条件
sodium cyanide; manganese(IV) oxide T=0 - 25°C; 28 h;
参考文献
Valdez-Padilla, David; Rodriguez-Morales, Sergio; Hernandez-Campos, Alicia; Hernandez-Luis, Francisco; Yepez-Mulia, Lilian; Tapia-Contreras, Amparo; Castillo, Rafael
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 4 p. 1724 - 1730
反应条件
sodium cyanide; manganese(IV) oxide; ammonia in isopropyl alcohol
T=0 - 25°C; 28 h;
参考文献
Valdez-Padilla, David; Rodriguez-Morales, Sergio; Hernandez-Campos, Alicia; Hernandez-Luis, Francisco; Yepez-Mulia, Lilian; Tapia-Contreras, Amparo; Castillo, Rafael
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 4 p. 1724 - 1730