N-(1-苄基-2-肼基-2-氧乙基)氨基甲酸叔丁酯合成路线 (共 6 条)
反应条件
hydrazine hydrate in methanol 18 h; Ambient temperature;
参考文献
Borg, Susanna; Estenne-Bouhtou, Genevieve; Luthman, Kristina; Csoeregh, Ingeborg; Hesselink, Willy; Hacksell, Uli
Journal of Organic Chemistry, 1995 , vol. 60, # 10 p. 3112 - 3120
反应条件
hydrazine hydrate in methanol 18 h;
参考文献
Matveeva; Kolesnikova; Zefirov
Russian Chemical Bulletin, 2011 , vol. 60, # 2 p. 248 - 253
反应条件
in ethanol; water T=20°C; 24 h;
参考文献
Da Costa, Cristiane F.; Pinheiro, Alessandra C.; De Almeida, Mauro V.; Lourenco, Maria C.S.; De Souza, Marcus V.N.
Chemical Biology and Drug Design, 2012 , vol. 79, # 2 p. 216 - 222
反应条件
hydrazine in tetrahydrofuran; methanol T=0 - 20°C;
参考文献
Liu, Zhuqing; Myers, Michael C.; Shah, Parag P.; Beavers, Mary Pat; Benedetti, Phillip A.; Diamond, Scott L.; Smith, Amos B.; Huryn, Donna M.
Combinatorial Chemistry and High Throughput Screening, 2010 , vol. 13, # 4 p. 337 - 351
反应条件
1: thionyl chloride / 24 h / 0 - 20 °C 2: triethylamine / tetrahydrofuran / 24 h / 20 °C 3: ethanol; water / 24 h / 20 °C View Scheme
参考文献
Da Costa, Cristiane F.; Pinheiro, Alessandra C.; De Almeida, Mauro V.; Lourenco, Maria C.S.; De Souza, Marcus V.N.
Chemical Biology and Drug Design, 2012 , vol. 79, # 2 p. 216 - 222
反应条件
1: triethylamine / tetrahydrofuran / 24 h / 20 °C 2: ethanol; water / 24 h / 20 °C View Scheme
参考文献
Da Costa, Cristiane F.; Pinheiro, Alessandra C.; De Almeida, Mauro V.; Lourenco, Maria C.S.; De Souza, Marcus V.N.
Chemical Biology and Drug Design, 2012 , vol. 79, # 2 p. 216 - 222