2-(4-异硫氰酸基苯基)乙醇合成路线 (共 3 条)
反应条件
trichlorosilane; triethylamine in benzene T=20°C; Elimination; 1 h;
参考文献
Zhang, Xuechun; Lee, Young K.; Kelley, James A.; Burke Jr., Terrence R.
Journal of Organic Chemistry, 2000 , vol. 65, # 19 p. 6237 - 6240
反应条件
in dichloromethane T=25°C; 24 h;
参考文献
Park, Soobong; Hayes, Brittany L.; Marankan, Fatima; Mulhearn, Debbie C.; Wanna, Linda; Mesecar, Andrew D.; Santarsiero, Bernard D.; Johnson, Michael E.; Venton, Duane L.
Journal of Medicinal Chemistry, 2003 , vol. 46, # 6 p. 936 - 953
反应条件
1: 75 percent / tetrahydrofuran / 0.5 h / 20 °C 2: 100 percent / Et3N; HSiCl3 / benzene / 1 h / 20 °C View Scheme
参考文献
Zhang, Xuechun; Lee, Young K.; Kelley, James A.; Burke Jr., Terrence R.
Journal of Organic Chemistry, 2000 , vol. 65, # 19 p. 6237 - 6240