N-甲氧基-N-甲基氨基甲酰氯合成路线 (共 14 条)
反应条件
pyridine in dichloromethane 1.) -78 deg C, 90 min, 2.) r.t.;
参考文献
Murakami, Masahiro; Hoshino, Yujiro; Ito, Hajime; Ito, Yoshihiko
Chemistry Letters, 1998 , # 2 p. 163 - 164
反应条件
triethylamine in diethyl ether T=-20 - -10°C; 1 h;
参考文献
Chervin, I. I.; Nasibov, Sh. S.; Rudchenko, V. F.; Shtamburg, V. G.; Kostyanovskii, R. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 3 p. 389 - 396
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 3 p. 544 - 552
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=60°C; 6 h;
参考文献
Murakami, Masahiro; Hoshino, Yujiro; Ito, Hajime; Ito, Yoshihiko
Chemistry Letters, 1998 , # 2 p. 163 - 164
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=60°C; 6 h;
参考文献
Murakami, Masahiro; Hoshino, Yujiro; Ito, Hajime; Ito, Yoshihiko
Chemistry Letters, 1998 , # 2 p. 163 - 164
反应条件
bis-triphenylphosphine-palladium(II) chloride; tripotassium phosphate monohydrate in ethanol T=65°C; 1 h; Inert atmosphere;
参考文献
Krishnamoorthy, Ravi; Lam, Sang Q.; Manley, Christopher M.; Herr, R. Jason
Journal of Organic Chemistry, 2010 , vol. 75, # 4 p. 1251 - 1258
反应条件
bis-triphenylphosphine-palladium(II) chloride; sodium carbonate in ethanol T=65°C; 2 h; Inert atmosphere;
参考文献
Krishnamoorthy, Ravi; Lam, Sang Q.; Manley, Christopher M.; Herr, R. Jason
Journal of Organic Chemistry, 2010 , vol. 75, # 4 p. 1251 - 1258
反应条件
bis-triphenylphosphine-palladium(II) chloride; tripotassium phosphate monohydrate in ethanol T=65°C; 1 h; Inert atmosphere;
参考文献
Krishnamoorthy, Ravi; Lam, Sang Q.; Manley, Christopher M.; Herr, R. Jason
Journal of Organic Chemistry, 2010 , vol. 75, # 4 p. 1251 - 1258
反应条件
bis-triphenylphosphine-palladium(II) chloride; tripotassium phosphate monohydrate in ethanol T=65°C; 1.5 h; Inert atmosphere;
参考文献
Krishnamoorthy, Ravi; Lam, Sang Q.; Manley, Christopher M.; Herr, R. Jason
Journal of Organic Chemistry, 2010 , vol. 75, # 4 p. 1251 - 1258
反应条件
bis-triphenylphosphine-palladium(II) chloride; tripotassium phosphate monohydrate in toluene T=80°C; 4 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 75, # 4 p. 1251 - 1258
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran
T=60°C; 6 h;
参考文献
Murakami, Masahiro; Hoshino, Yujiro; Ito, Hajime; Ito, Yoshihiko
Chemistry Letters, 1998 , # 2 p. 163 - 164