(S)-(-)-2-异氰酰基-3-甲基丁酸合成路线 (共 5 条)
反应条件
pyridine in tetrahydrofuran; dichloromethane T=0°C; 2 h;
参考文献
Nowick, James S.; Powell, Noel A.; Nguyen, Tram M.; Noronha, Glenn
Journal of Organic Chemistry, 1992 , vol. 57, # 28 p. 7364 - 7366
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 59, # 7 p. 1937 - 1938
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane T=25°C; 0.166667 h;
参考文献
Knoelker, Hans-Joachim; Braxmeier, Tobias
Synlett, 1997 , vol. 1997, # 8 p. 925 - 928
反应条件
in toluene 1 h; Heating;
参考文献
Oberhoff, Markus; Erker, Gerhard; Froehlich, Roland
Chemistry - A European Journal, 1997 , vol. 3, # 9 p. 1521 - 1525
反应条件
1: acetyl chloride / Reflux 2: sodium hydrogencarbonate / dichloromethane / 0.25 h / Cooling with ice View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 20, # 12 p. 3807 - 3815