反应条件
1: (S)-1-ethyl-2-(p-tolylsulfinyl)benzene With n-butyllithium; diisopropylamine in tetrahydrofuran; hexane T=-78 - 0°C; Cooling; 2: With copper (I) cyanide; lithium chloride in tetrahydrofuran; hexane T=-78°C; 0.0833333 h; Cooling; 3: 4-phenylbut-3-yn-2-yl methanesulfonate in tetrahydrofuran; hexane T=-78°C; 0.0833333 h; optical yield given as percent de;
参考文献
Angewandte Chemie - International Edition, , vol. 47, # 36 p. 6836 - 6839