2-甲氧基-N,N-二甲基乙胺合成路线 (共 11 条)
反应条件
formic acid in water T=0 - 80°C;
参考文献
Remenar, Julius F.; Lucht, Brett L.; Collum, David B.
Journal of the American Chemical Society, 1997 , vol. 119, # 24 p. 5567 - 5572
反应条件
formic acid in water Eschweiler-Clarke reaction; 16 h; Heating;
参考文献
Bilke, Julia L.; O'Brien, Peter
Journal of Organic Chemistry, 2008 , vol. 73, # 16 p. 6452 - 6454
反应条件
in water T=40°C; 24 h;
参考文献
Chen, Zhengjian; Liu, Shimin; Li, Zuopeng; Zhang, Qinghua; Deng, Youquan
New Journal of Chemistry, 2011 , vol. 35, # 8 p. 1596 - 1606
反应条件
in methanol Heating;
参考文献
Di Vona, Maria Luisa; Illuminati, Gabriello; Lillocci, Claudio
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 1943 - 1946
反应条件
in toluene; pentane T=-80°C; Equilibrium constant;
参考文献
Remenar, Julius F.; Lucht, Brett L.; Collum, David B.
Journal of the American Chemical Society, 1997 , vol. 119, # 24 p. 5567 - 5572
参考文献
Clarke
Journal of the Chemical Society, 1912 , vol. 101, p. 1804
反应条件
sodium hydride 1.) THF, room temp., 1 h; 2.) room temp., 1 h; Yield given. Multistep reaction;
参考文献
Kashima, Choji; Harada, Kazuo; Omote, Yoshimori
Canadian Journal of Chemistry, 1985 , vol. 63, p. 288 - 290
反应条件
in methanol T=-20°C; other temp.; ΔH(excit.), ΔS(excit.); Rate constantThermodynamic data;
参考文献
Vona, Maria Luisa Di; Illuminati, Gabriello; Lillocci, Claudio
Journal of the Chemical Society, Chemical Communications, 1985 , # 7 p. 380 - 381
反应条件
in methanol T=130°C; Rate constantThermodynamic data;
参考文献
Di Vona, Maria Luisa; Illuminati, Gabriello; Lillocci, Claudio
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 1943 - 1946
反应条件
(batho)2CuII (batho = 2,9-dimethyl-4,7-diphenyl-1,10-phenanthrolinedisulfonate); water T=25°C; 24 h; pH 8; Rate constant;
参考文献
Wang, Fengjiang; Sayre, Lawrence M.
Journal of the American Chemical Society, 1992 , vol. 114, # 1 p. 248 - 255