1,2,3,4-四甲基萘合成路线 （共 49 条）
参考文献
Sekiguchi, Akira; Zigler, Steven S.; Haller, Kenneth J.; West, Robert
Recueil des Travaux Chimiques des Pays-Bas, 1988 , vol. 107, # 3 p. 197 - 202
反应条件
1: 76 percent / tetraethylammonium bromide; CuBr; triethylamine / 100 °C / 167200 Torr 2: 91 percent / polyphosphoric acid / 0.5 h / 80 °C 3: 20 percent / LiAlH4 / dioxane / 8 h / Heating View Scheme
参考文献
Chudinov; Gashev; Chernysheva; Semenov
Russian Chemical Bulletin, 2006 , vol. 55, # 1 p. 123 - 136
反应条件
1: 91 percent / polyphosphoric acid / 0.5 h / 80 °C 2: 20 percent / LiAlH4 / dioxane / 8 h / Heating View Scheme
参考文献
Chudinov; Gashev; Chernysheva; Semenov
Russian Chemical Bulletin, 2006 , vol. 55, # 1 p. 123 - 136
反应条件
1: 71 percent / ammonia; KOH / ethanol / 20 °C 2: 76 percent / tetraethylammonium bromide; CuBr; triethylamine / 100 °C / 167200 Torr 3: 91 percent / polyphosphoric acid / 0.5 h / 80 °C 4: 20 percent / LiAlH4 / dioxane / 8 h / Heating View Scheme
参考文献
Chudinov; Gashev; Chernysheva; Semenov
Russian Chemical Bulletin, 2006 , vol. 55, # 1 p. 123 - 136
反应条件
hydrogen bromide; acetic acid in chloroform
参考文献
Staab,H.A. et al.
Chemische Berichte, 1978 , vol. 111, p. 2965 - 2981
反应条件
palladium T=225 - 230°C;
参考文献
Shishido; Nozaki
Journal of the American Chemical Society, 1947 , vol. 69, p. 963
Kogyo Kagaku Zasshi, 1944 , vol. 47, p. 900
Chem.Abstr., 1948 , p. 6791
反应条件
1: 84 percent / polyphosphoric acid / 0.5 h / 80 °C 2: 100 percent / KOH / methanol; H2O / 10 h / Heating View Scheme
参考文献
Chudinov; Gashev; Chernysheva; Semenov
Russian Chemical Bulletin, 2006 , vol. 55, # 1 p. 123 - 136
反应条件
1: 96 percent / magnesium / tetrahydrofuran 2: 87 percent / benzene / 2 h / 350 °C View Scheme
参考文献
Sekiguchi, Akira; Zigler, Steven S.; Haller, Kenneth J.; West, Robert
Recueil des Travaux Chimiques des Pays-Bas, 1988 , vol. 107, # 3 p. 197 - 202
反应条件
1: N2H4*H2O, NaOH / bis-(2-hydroxy-ethyl) ether 2: TiCl4 / CH2Cl2 3: N2H4*H2O, NaOH / bis-(2-hydroxy-ethyl) ether View Scheme
参考文献
Aslam,F.M. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1972 , p. 892 - 894
反应条件
1: (rearrangement) / 1,2-dichloro-benzene / 150 °C 2: Mg, BrCH2CH2Br 3: OsO4, Py 4: Pb(OAc)4 5: N2H4*H2O, KOH View Scheme
参考文献
Criegee,R. et al.
Chemische Berichte, 1970 , vol. 103, p. 960 - 972
