2,2-二甲基-1-(4-甲基苯基)丙-1-酮合成路线 （共 30 条）
反应条件
carbon monoxide in tetrahydrofuran; diethyl ether; Petroleum ether T=-110°C;
参考文献
Journal of Organic Chemistry, , vol. 58, # 21 p. 5843 - 5845
反应条件
in 1,2-dichloro-benzene T=180°C; 4 h; Inert atmosphere;
参考文献
Lo Fiego, Marcos J.; Lockhart, Maria T.; Chopa, Alicia B.
Journal of Organometallic Chemistry, 2009 , vol. 694, # 22 p. 3674 - 3678
参考文献
Journal of the American Chemical Society, , vol. 72, p. 876
反应条件
iodine 0.25 h; Ambient temperatureIrradiation;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 35, # 11 p. 1197 - 1198
反应条件
1: toluene 2: aqueous HCl View Scheme
参考文献
Journal of the American Chemical Society, , vol. 72, p. 876
反应条件
diethyl ether anschliessend mit wss.HCl;
参考文献
Journal of the American Chemical Society, , vol. 72, p. 4169
反应条件
aluminium trichloride in dichloromethane T=20°C; 0.5 h; Yield given;
参考文献
Tetrahedron, , vol. 45, # 4 p. 951 - 960
反应条件
1.1: potassium tert-butylate / isopropyl alcohol / Inert atmosphere 2.1: 1,1'-bis-(diphenylphosphino)ferrocene; 1,10-phenanthroline; Pd(F6-acac)2; cyclohexylamine; copper(I) bromide / quinoline / 36 h / 100 °C / Inert atmosphere; Molecular sieve 2.2: 1 h / 80 °C / Inert atmosphere View Scheme
参考文献
European Journal of Organic Chemistry, , # 32 p. 6486 - 6501
反应条件
C10H16NO5; potassium carbonate; bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane T=20°C;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 31 p. 8093 - 8097
Angew. Chem., , vol. 125, # 31 p. 8251 - 8255,5
反应条件
1.1: Lawesson reagent / CH2Cl2 / 20 °C 1.2: CH2Cl2 / 20 °C 2.1: Lawesson reagent / CH2Cl2 / 1 h / 20 °C 2.2: 12 mg / CH2Cl2 / 72 h / 20 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 77, # 1 p. 187 - 188
