2H-全氟(2-甲基戊烷)合成路线 （共 72 条）
反应条件
bis [2-(2-methoxyethoxy)ethyl] ether; trifluoroacetic acid T=-30 - 0°C; 0.5 h;
参考文献
Smart, Bruce E.; Middleton, William J.; Farnham, William B.
Journal of the American Chemical Society, 1986 , vol. 108, # 16 p. 4905 - 4907
反应条件
hydrazine hydrate; trifluoroacetic acid in ethylene glycol dimethyl ether Ambient temperature;
参考文献
Bargamova, M. D.; Bargamov, G. G.; German, L. S.
Journal of Fluorine Chemistry, 1993 , vol. 65, # 3 p. 213 - 216
反应条件
in ethyl acetate T=80°C; 12 h;
参考文献
Rozhkov, I. N.; Chaplina, I. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 12 p. 2451 - 2456
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , vol. 40, # 12 p. 2810 - 2815
反应条件
triethylamine in diethyl ether T=20°C; 2 h; Yields of byproduct given;
参考文献
Snegirev, V. F.; Makarov, K. N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 1 p. 91 - 103
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 1 p. 106 - 119
反应条件
4-oxo-1,4-dihydropyridine in acetone 6 h; Ambient temperature;
参考文献
Yanagida, Shozo; Noji, Yukihiro; Okahara, Mitsuo
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 4 p. 1151 - 1158
反应条件
pyridine; 1,1,1,3,3,3-hexamethyl-disilazane in acetonitrile 4 h; Heating;
参考文献
Furin; Zhuzhgov
Russian Journal of General Chemistry, 1998 , vol. 68, # 1 p. 38 - 43
反应条件
tris(2-methoxyethyl)amine; water in N,N-dimethyl-formamide
参考文献
Dmowski, Wojciech; Wozniacki, Ryszard
Journal of Fluorine Chemistry, 1985 , vol. 29, p. 126
反应条件
18-crown-6 ether; potassium carbonate in dichloromethane 24 h; Ambient temperature;
参考文献
Yanagida, Shozo; Noji, Yukihiro; Okahara, Mitsuo
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 4 p. 1151 - 1158
反应条件
cesium fluoride; 1,1,1,3,3,3-hexamethyl-disilazane in N,N-dimethyl-formamide T=50°C; 1 h;
参考文献
Cheburkov, Yuri; Moore, George G.I.
Journal of Fluorine Chemistry, 2003 , vol. 123, # 2 p. 227 - 231
反应条件
in tetrahydrofuran T=0°C; Addition; Cyclization; 1 h;
参考文献
Furin; Kiriyanko; Zhuzhgov
Russian Journal of Organic Chemistry, 2000 , vol. 36, # 1 p. 24 - 29
