2H-全氟(2-甲基戊烷)合成路线 （共 72 条）
反应条件
triethylamine in acetonitrile T=0 - 5°C; Addition; Cyclization; 1 h;
参考文献
Furin; Kiriyanko; Zhuzhgov
Russian Journal of Organic Chemistry, 2000 , vol. 36, # 1 p. 24 - 29
反应条件
perfluoro-4-methyl-2-pentene; cesium fluoride in N,N-dimethyl-formamide T=60°C; 18 h;
参考文献
Dmowski, Wojciech; Wozniacki, Ryszard
Journal of Fluorine Chemistry, 1987 , vol. 36, p. 385 - 394
反应条件
3-iodo-1,1,1-trifluoropropane; cesium fluoride in N,N-dimethyl-formamide T=60°C; 18 h;
参考文献
Dmowski, Wojciech; Wozniacki, Ryszard
Journal of Fluorine Chemistry, 1987 , vol. 36, p. 385 - 394
反应条件
ammonia in diethyl ether T=20°C; 3 h; Yield given. Yields of byproduct given;
参考文献
Zeifman, Yu. V.; German, L. S.
Russian Chemical Bulletin, 1994 , vol. 43, # 9 p. 1588 - 1590
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1994 , # 9 p. 1678 - 1679
反应条件
methanol; triethylamine in acetonitrile T=45°C; 5 h; Yield given. Yields of byproduct given;
参考文献
Moldavskii; Bispen; Furin; Zhuzhgov
Russian Journal of Applied Chemistry, 1996 , vol. 69, # 4 p. 575 - 582
反应条件
1: CsF / bis-(2-methoxy-ethyl) ether / 3 h / 200 °C 2: Et3N / diethyl ether / 2 h / 20 °C View Scheme
参考文献
Snegirev, V. F.; Makarov, K. N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 1 p. 91 - 103
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 1 p. 106 - 119
反应条件
cesium fluoride in N,N-dimethyl-formamide T=18°C; 48 h; Yields of byproduct given;
参考文献
Dmowski, Wojciech; Wozniacki, Ryszard
Journal of Fluorine Chemistry, 1987 , vol. 36, p. 385 - 394
反应条件
cesium fluoride in N,N-dimethyl-formamide T=18°C; 48 h; Yields of byproduct given;
参考文献
Dmowski, Wojciech; Wozniacki, Ryszard
Journal of Fluorine Chemistry, 1987 , vol. 36, p. 385 - 394
反应条件
cesium fluoride in N,N-dimethyl-formamide T=60°C; 18 h; Yields of byproduct given;
参考文献
Dmowski, Wojciech; Wozniacki, Ryszard
Journal of Fluorine Chemistry, 1987 , vol. 36, p. 385 - 394
反应条件
potassium fluoride in N,N-dimethyl-formamide T=60°C; 36 h; Yields of byproduct given;
参考文献
Dmowski, Wojciech; Wozniacki, Ryszard
Journal of Fluorine Chemistry, 1987 , vol. 36, p. 385 - 394
