2H-全氟(2-甲基戊烷)合成路线 （共 72 条）
反应条件
bis(.eta.(6)-benzene)chromium in pyridine 72 h; Yield given. Yields of byproduct given;
参考文献
Huang,Y.; Zhou,J.; Zhu,Z.
Journal of Fluorine Chemistry, 1986 , vol. 30, p. 455
反应条件
bis(.eta.(6)-benzene)chromium in pyridine 72 h; Yield given. Yields of byproduct given;
参考文献
Huang,Y.; Zhou,J.; Zhu,Z.
Journal of Fluorine Chemistry, 1986 , vol. 30, p. 455
反应条件
triethylamine T=55 - 60°C; 23 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Cheburkov, Yuri; Moore, George G.I.
Journal of Fluorine Chemistry, 2003 , vol. 123, # 2 p. 227 - 231
反应条件
1: With triethylamine T=55 - 60°C; 23 h; 2: With potassium hydroxide Heating;
参考文献
Cheburkov, Yuri; Moore, George G.I.
Journal of Fluorine Chemistry, 2003 , vol. 123, # 2 p. 227 - 231
反应条件
1: F(1-) 2: F(1-) View Scheme
参考文献
Dmowski, Wojciech; Wozniacki, Ryszard
Journal of Fluorine Chemistry, 1985 , vol. 29, p. 126
反应条件
in diethyl ether T=20°C; 2 h; Further byproducts given. Yields of byproduct given;
参考文献
Snegirev, V. F.; Makarov, K. N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 1 p. 91 - 103
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 1 p. 106 - 119
反应条件
lithium iodide in acetonitrile T=0°C; 0.5 h; also with LiBr, variation of time and temperature; Product distributionMechanism;
参考文献
Blume, Elisabeth; Gasafi-Martin, Waltraud; Probst, Anton; Werner, Konrad von
Journal of Fluorine Chemistry, 1991 , vol. 53, # 3 p. 387 - 396
反应条件
tetrabutylammomium bromide in 1,2-dichloro-ethane T=20°C; var. nucleophiles and aolvents; Product distributionMechanism;
参考文献
Rozhkov, I. N.; Chaplina, I. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 12 p. 2451 - 2456
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , vol. 40, # 12 p. 2810 - 2815
反应条件
lithium bromide in acetonitrile T=0°C; 0.25 h; also with LiI and LiCl, variation of time; Product distributionMechanism;
参考文献
Blume, Elisabeth; Gasafi-Martin, Waltraud; Probst, Anton; Werner, Konrad von
Journal of Fluorine Chemistry, 1991 , vol. 53, # 3 p. 387 - 396
反应条件
boron trifluoride diethyl etherate in diethyl ether T=-37°C; other reagents or without ones; different solvents and temperatures; Product distribution;
参考文献
Ono, Taizo; Yamanouchi, Kouichi; Scherer, Kirby V.
Journal of Fluorine Chemistry, 1995 , vol. 73, # 2 p. 267 - 272
