2H-全氟(2-甲基戊烷)合成路线 (共 72 条)
反应条件
tetrabutylammomium bromide in ethyl acetate T=20°C; 72 h; other alkenes, alkynes, and butadiene; var. solvents, nucleophiles, and temperature; Product distributionMechanism;
参考文献
Rozhkov, I. N.; Chaplina, I. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 12 p. 2451 - 2456
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , vol. 40, # 12 p. 2810 - 2815
反应条件
triethylamine in acetonitrile T=0°C; 1 h; other fluorinated compounds, dependence on reagents and reaction conditions; Product distribution;
参考文献
Moldavskii; Bispen; Furin; Zhuzhgov
Russian Journal of Applied Chemistry, 1996 , vol. 69, # 4 p. 575 - 582
反应条件
triethylamine in diethyl ether T=20°C; 2 h; reactiohn with various oxygen nucleophiles, effect of reagent concentration; Product distribution;
参考文献
Snegirev, V. F.; Makarov, K. N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 1 p. 91 - 103
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 1 p. 106 - 119
反应条件
24 h; Ambient temperature;
参考文献
Ikeda, Isao; Tsukamoto, Takeo; Okahara, Mitsuo
Chemistry Letters, 1980 , p. 583 - 586
参考文献
Dmowski, Wojciech; Wozniacki, Ryszard
Journal of Fluorine Chemistry, 1985 , vol. 29, p. 126
参考文献
Dmowski, Wojciech; Wozniacki, Ryszard
Journal of Fluorine Chemistry, 1985 , vol. 29, p. 126
反应条件
in tetrahydrofuran 24 h; Ambient temperature;
参考文献
Ikeda, Isao; Tsukamoto, Takeo; Okahara, Mitsuo
Chemistry Letters, 1980 , p. 583 - 586
反应条件
1: With triethylamine; tert-butyl alcohol T=55 - 60°C; 20 h; 2: With toluene-4-sulfonic acid T=115°C; 3 h; 3: With water; triethylamine Heating; Title compound not separated from byproducts;
参考文献
Cheburkov, Yuri; Moore, George G.I.
Journal of Fluorine Chemistry, 2003 , vol. 123, # 2 p. 227 - 231
反应条件
chlorine; triethylamine
参考文献
Sud'enkov,Yu.Ya.
Journal of Organic Chemistry USSR (English Translation), 1978 , vol. 14, p. 1240 - 1241
Zhurnal Organicheskoi Khimii, 1978 , vol. 14, # 6 p. 1336 - 1337
反应条件
in diethyl ether
T=20°C; 14 h; Yield given. Yields of byproduct given;
参考文献
Snegirev, V. F.; Zakharova, E. V.; Makarov, K. N.; Knunyants, I. L.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 11 p. 2305 - 2312
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 11 p. 2561 - 2568