反应条件
1: 1.) n-BuLi / 1.) THF, a) -78 deg C, 0.5 h, b) 0 deg C, 0.1 h, 2.) THF, a) -78 deg C, 1 h, b) 0 deg C, 1 h
2: 85 percent / KBH4 / methanol / Ambient temperature
3: 68 percent / 15percent aq. HCl / 72 h / Ambient temperature
View Scheme
参考文献
Epsztajn; Jozwiak; Szczesniak
Synthetic Communications, 1994 , vol. 24, # 13 p. 1789 - 1798
