2,4-二氨基-6-(4-甲氧苯基)-1,3,5-三嗪合成路线 (共 5 条)
反应条件
potassium hydroxide in pentan-1-ol T=140°C; 24 h;
参考文献
Deans, Robert; Cooke, Graeme; Rotello, Vincent M.
Journal of Organic Chemistry, 1997 , vol. 62, # 4 p. 836 - 839
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether Suzuki cross-coupling reaction; Heating;
参考文献
Cooke; Augier de Cremiers; Rotello; Tarbit; Vanderstraeten
Tetrahedron, 2001 , vol. 57, # 14 p. 2787 - 2789
反应条件
1: 4-methoxy-benzaldehyde With ammonia; iodine in tetrahydrofuran; water T=20°C; 1 h; 2: 1-cyano-guanidine With potassium hydroxide in tetrahydrofuran; water 48 h; Heating; Further stages.;
参考文献
Shie, Jiun-Jie; Fang, Jim-Min
Journal of Organic Chemistry, 2003 , vol. 68, # 3 p. 1158 - 1160
反应条件
1: aq. NH3; iodine / tetrahydrofuran / 1 h / 25 °C 2: tetrahydrofuran; H2O / 80 °C / microwave irradiation View Scheme
参考文献
Journal of Organic Chemistry, , vol. 72, # 8 p. 3141 - 3144
反应条件
1: ueber die Diazonium-Verbindung dargestellt View Scheme
参考文献
Monatshefte fuer Chemie, , vol. 79, p. 106,111