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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
30358-99-7
合成路线
（共 63 条）
836-43-1
4-苄氧基苄醇
→
反应条件
30358-99-7
反应条件
1: TMSBr 2: toluene / 0.33 h / Heating 3: 96 percent / n-BuLi / tetrahydrofuran; hexane / 0.5 h / 0 °C 4: 93 percent / H2 / Pd/Al2O3 / tetrahydrofuran / 4 h / 20 °C / 37503 Torr View Scheme
参考文献
Colobert, Francoise; Mazery, Renaud Des; Solladie, Guy; Carreno, M Carmen
Organic letters, 2002 , vol. 4, # 10 p. 1723 - 1725
436806-94-9
→
反应条件
30358-99-7
反应条件
1: 96 percent / n-BuLi / tetrahydrofuran; hexane / 0.5 h / 0 °C 2: 93 percent / H2 / Pd/Al2O3 / tetrahydrofuran / 4 h / 20 °C / 37503 Torr View Scheme
参考文献
Colobert, Francoise; Mazery, Renaud Des; Solladie, Guy; Carreno, M Carmen
Organic letters, 2002 , vol. 4, # 10 p. 1723 - 1725
7448-86-4
→
反应条件
30358-99-7
反应条件
1: 78 percent / second generation Grubbs' catalyst / CH2Cl2 / 12 h / 40 °C 2: 95 percent / H2 / RhCl(PPh3)3 / benzene / 4 h / 20 °C 3: 90 percent / Et3SiH; BiBr3 / acetonitrile / 1 h / 20 °C 4: 41.0 mg / TBAF / acetonitrile; tetrahydrofuran / 0.17 h View Scheme
参考文献
Evans, P. Andrew; Cui, Jian; Gharpure, Santosh J.
Organic Letters, 2003 , vol. 5, # 21 p. 3883 - 3885
147974-20-7
→
反应条件
30358-99-7
反应条件
1: (R)-BINOL; 4 Angstroem molecular sieves; Ti(OPr-i)4 / CH2Cl2 / 96 h / -20 °C 2: 99 percent / 2,6-lutidine / CH2Cl2 / 0 - 20 °C 3: 78 percent / second generation Grubbs' catalyst / CH2Cl2 / 12 h / 40 °C 4: 95 percent / H2 / RhCl(PPh3)3 / benzene / 4 h / 20 °C 5: 90 percent / Et3SiH; BiBr3 / acetonitrile / 1 h / 20 °C 6: 41.0 mg / TBAF / acetonitrile; tetrahydrofuran / 0.17 h View Scheme
参考文献
Evans, P. Andrew; Cui, Jian; Gharpure, Santosh J.
Organic Letters, 2003 , vol. 5, # 21 p. 3883 - 3885
622397-33-5
→
反应条件
30358-99-7
反应条件
1: 99 percent / 2,6-lutidine / CH2Cl2 / 0 - 20 °C 2: 78 percent / second generation Grubbs' catalyst / CH2Cl2 / 12 h / 40 °C 3: 95 percent / H2 / RhCl(PPh3)3 / benzene / 4 h / 20 °C 4: 90 percent / Et3SiH; BiBr3 / acetonitrile / 1 h / 20 °C 5: 41.0 mg / TBAF / acetonitrile; tetrahydrofuran / 0.17 h View Scheme
参考文献
Evans, P. Andrew; Cui, Jian; Gharpure, Santosh J.
Organic Letters, 2003 , vol. 5, # 21 p. 3883 - 3885
622397-17-5
→
反应条件
30358-99-7
反应条件
1: 78 percent / second generation Grubbs' catalyst / CH2Cl2 / 12 h / 40 °C 2: 95 percent / H2 / RhCl(PPh3)3 / benzene / 4 h / 20 °C 3: 90 percent / Et3SiH; BiBr3 / acetonitrile / 1 h / 20 °C 4: 41.0 mg / TBAF / acetonitrile; tetrahydrofuran / 0.17 h View Scheme
参考文献
Evans, P. Andrew; Cui, Jian; Gharpure, Santosh J.
Organic Letters, 2003 , vol. 5, # 21 p. 3883 - 3885
622397-34-6
→
反应条件
30358-99-7
反应条件
1: 95 percent / H2 / RhCl(PPh3)3 / benzene / 4 h / 20 °C 2: 90 percent / Et3SiH; BiBr3 / acetonitrile / 1 h / 20 °C 3: 41.0 mg / TBAF / acetonitrile; tetrahydrofuran / 0.17 h View Scheme
参考文献
Evans, P. Andrew; Cui, Jian; Gharpure, Santosh J.
Organic Letters, 2003 , vol. 5, # 21 p. 3883 - 3885
477284-13-2
→
反应条件
30358-99-7
反应条件
1: 89 percent / SnBr4 / CH2Cl2 / 1 h / -78 °C 2: 72 percent / Bu3SnH / AIBN / toluene / 0.5 h / Heating 3: 82 percent / 2-(di-tert-butylphosphino)biphenyl / Pd2(dba)3 / toluene / 24 h / 110 °C 4: TFA / CH2Cl2 / 1 h / 0 - 20 °C 5: K2CO3 / acetone / 12 h / 20 °C 6: 72 percent / H2 / 10percent Pd/C / methanol; ethyl acetate / 7 h / 20 °C View Scheme
参考文献
Marumoto, Shinji; Jaber, James J; Vitale, Justin P; Rychnovsky, Scott D
Organic letters, 2002 , vol. 4, # 22 p. 3919 - 3922
477284-12-1
→
反应条件
30358-99-7
反应条件
1: 93 percent / DIBAL-H; pyridine; DMAP / CH2Cl2; hexane / -78 - 0 °C 2: 89 percent / SnBr4 / CH2Cl2 / 1 h / -78 °C 3: 72 percent / Bu3SnH / AIBN / toluene / 0.5 h / Heating 4: 82 percent / 2-(di-tert-butylphosphino)biphenyl / Pd2(dba)3 / toluene / 24 h / 110 °C 5: TFA / CH2Cl2 / 1 h / 0 - 20 °C 6: K2CO3 / acetone / 12 h / 20 °C 7: 72 percent / H2 / 10percent Pd/C / methanol; ethyl acetate / 7 h / 20 °C View Scheme
参考文献
Marumoto, Shinji; Jaber, James J; Vitale, Justin P; Rychnovsky, Scott D
Organic letters, 2002 , vol. 4, # 22 p. 3919 - 3922
50463-48-4
3-[4-(苄氧基)苯基]丙酸
→
反应条件
30358-99-7
反应条件
1: 94 percent / DCC / DMAP / CH2Cl2 / 12 h / 20 °C 2: DIBAL-H / -78 °C 3: DMAP; pyridine; DIBAL-H / CH2Cl2; hexane / -78 - 0 °C 4: 84 percent / SnBr4 / CH2Cl2 / 1.3 h / -78 °C 5: K2CO3 / methanol / 3 h / Heating 6: 217 mg / K2CO3 / acetone / 12 h 7: 86 percent / Bu3SnH; AIBN / toluene / 0.25 h / Heating 8: 72 percent / H2 / 10percent Pd/C / methanol; ethyl acetate / 7 h / 20 °C View Scheme
参考文献
Marumoto, Shinji; Jaber, James J; Vitale, Justin P; Rychnovsky, Scott D
Organic letters, 2002 , vol. 4, # 22 p. 3919 - 3922
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