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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
30358-99-7
合成路线
（共 63 条）
5544-60-5
4-苄氧基溴苄
→
反应条件
30358-99-7
反应条件
1: toluene / 0.33 h / Heating 2: 96 percent / n-BuLi / tetrahydrofuran; hexane / 0.5 h / 0 °C 3: 93 percent / H2 / Pd/Al2O3 / tetrahydrofuran / 4 h / 20 °C / 37503 Torr View Scheme
参考文献
Colobert, Francoise; Mazery, Renaud Des; Solladie, Guy; Carreno, M Carmen
Organic letters, 2002 , vol. 4, # 10 p. 1723 - 1725
612806-38-9
→
反应条件
30358-99-7
反应条件
1: 81 percent / 4 Angstroem molecular sieves; Celite; PCC / CH2Cl2 / 3 h / 20 °C 2: 96 percent / n-BuLi / tetrahydrofuran; hexane / 0.5 h / 0 °C 3: 93 percent / H2 / Pd/Al2O3 / tetrahydrofuran / 4 h / 20 °C / 37503 Torr View Scheme
参考文献
Carreno, M. Carmen; Des Mazery, Renaud; Urbano, Antonio; Colobert, Francoise; Solladie, Guy
Journal of Organic Chemistry, 2003 , vol. 68, # 20 p. 7779 - 7787
1026305-29-2
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反应条件
30358-99-7
反应条件
1.1: aq. K2CO3 / acetonitrile / 0.5 h / 20 °C 1.2: aq. NaBH4 / acetonitrile / 1 h / 20 °C 2.1: 81 percent / 4 Angstroem molecular sieves; Celite; PCC / CH2Cl2 / 3 h / 20 °C 3.1: 96 percent / n-BuLi / tetrahydrofuran; hexane / 0.5 h / 0 °C 4.1: 93 percent / H2 / Pd/Al2O3 / tetrahydrofuran / 4 h / 20 °C / 37503 Torr View Scheme
参考文献
Carreno, M. Carmen; Des Mazery, Renaud; Urbano, Antonio; Colobert, Francoise; Solladie, Guy
Journal of Organic Chemistry, 2003 , vol. 68, # 20 p. 7779 - 7787
767330-08-5
→
反应条件
30358-99-7
反应条件
triethylsilane; boron trifluoride diethyl etherate in dichloromethane T=-78 - 20°C;
参考文献
Boulard, Lucie; Bouzbouz, Samir; Cossy, Janine; Franck, Xavier; Figadere, Bruno
Tetrahedron Letters, 2004 , vol. 45, # 35 p. 6603 - 6605
123-11-5
大茴香醛
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反应条件
30358-99-7
反应条件
1: 70 percent / InCl3 / CH2Cl2 / 22 h / 0 °C 2: 70 percent / Bu3SnH; 1,1'-azobis(cyclohexane carbonitrile) / benzene / 16 h / Heating 3: H2 / Pd/C / methanol; ethyl acetate / 3 h / 20 °C View Scheme
参考文献
Lee, Cheng-Hsia Angeline; Loh, Teck-Peng
Tetrahedron Letters, 2006 , vol. 47, # 10 p. 1641 - 1644
866412-24-0
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反应条件
30358-99-7
反应条件
1.1: 73 percent / K2CO3 / acetone / 4 h / Heating 2.1: O3 / CH2Cl2 / 1 h / -78 °C 2.2: TPP / CH2Cl2 3.1: CH2Cl2 / 2 h / 20 °C 4.1: 81 percent / Mg / 3 h / 20 °C 5.1: 76 percent / LAH / tetrahydrofuran / 3 h / 0 - 20 °C 6.1: 80 percent / IBX / dimethylsulfoxide / 4 h / 20 °C 7.1: 81 percent / Ba(OH)2*8H2O / tetrahydrofuran; H2O / 5 h / 20 °C 8.1: 80 percent / HF*Py / tetrahydrofuran / 4 h / Heating 9.1: 70 percent / H2; HCl / Pd/C / ethanol; ethyl acetate; H2O / 10 h View Scheme
参考文献
Chandrasekhar; Jaya Prakash; Shyamsunder
Tetrahedron Letters, 2005 , vol. 46, # 39 p. 6651 - 6653
866412-16-0
→
反应条件
30358-99-7
反应条件
1.1: O3 / CH2Cl2 / 1 h / -78 °C 1.2: TPP / CH2Cl2 2.1: CH2Cl2 / 2 h / 20 °C 3.1: 81 percent / Mg / 3 h / 20 °C 4.1: 76 percent / LAH / tetrahydrofuran / 3 h / 0 - 20 °C 5.1: 80 percent / IBX / dimethylsulfoxide / 4 h / 20 °C 6.1: 81 percent / Ba(OH)2*8H2O / tetrahydrofuran; H2O / 5 h / 20 °C 7.1: 80 percent / HF*Py / tetrahydrofuran / 4 h / Heating 8.1: 70 percent / H2; HCl / Pd/C / ethanol; ethyl acetate; H2O / 10 h View Scheme
参考文献
Chandrasekhar; Jaya Prakash; Shyamsunder
Tetrahedron Letters, 2005 , vol. 46, # 39 p. 6651 - 6653
866412-14-8
→
反应条件
30358-99-7
反应条件
1: 81 percent / Ba(OH)2*8H2O / tetrahydrofuran; H2O / 5 h / 20 °C 2: 80 percent / HF*Py / tetrahydrofuran / 4 h / Heating 3: 70 percent / H2; HCl / Pd/C / ethanol; ethyl acetate; H2O / 10 h View Scheme
参考文献
Chandrasekhar; Jaya Prakash; Shyamsunder
Tetrahedron Letters, 2005 , vol. 46, # 39 p. 6651 - 6653
866412-19-3
→
反应条件
30358-99-7
反应条件
1: 80 percent / IBX / dimethylsulfoxide / 4 h / 20 °C 2: 81 percent / Ba(OH)2*8H2O / tetrahydrofuran; H2O / 5 h / 20 °C 3: 80 percent / HF*Py / tetrahydrofuran / 4 h / Heating 4: 70 percent / H2; HCl / Pd/C / ethanol; ethyl acetate; H2O / 10 h View Scheme
参考文献
Chandrasekhar; Jaya Prakash; Shyamsunder
Tetrahedron Letters, 2005 , vol. 46, # 39 p. 6651 - 6653
866412-18-2
→
反应条件
30358-99-7
反应条件
1: 76 percent / LAH / tetrahydrofuran / 3 h / 0 - 20 °C 2: 80 percent / IBX / dimethylsulfoxide / 4 h / 20 °C 3: 81 percent / Ba(OH)2*8H2O / tetrahydrofuran; H2O / 5 h / 20 °C 4: 80 percent / HF*Py / tetrahydrofuran / 4 h / Heating 5: 70 percent / H2; HCl / Pd/C / ethanol; ethyl acetate; H2O / 10 h View Scheme
参考文献
Chandrasekhar; Jaya Prakash; Shyamsunder
Tetrahedron Letters, 2005 , vol. 46, # 39 p. 6651 - 6653
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