(2E,4E)-2,4-癸二烯酸合成路线 （共 46 条）
反应条件
1: petroleum ether; thionyl chloride
View Scheme
参考文献
Jacobson
Journal of the American Chemical Society, 1953 , vol. 75, p. 2584 Anm. 11
参考文献
Arnone, Alberto; Cardillo, Rosanna; Nasini, Gianluca; Pava, Orso Vajna de; Quaroni, Sergio
Phytochemistry (Elsevier), 1988 , vol. 27, # 11 p. 3611 - 3618
参考文献
Crombie et al.
Journal of the Chemical Society, 1955 , p. 1025
反应条件
triethylamine; trichlorophosphate in dichloromethane
1) 0 deg C, 2 h, 2) room temperature, 1 h;
参考文献
Bari; Sattar; Vig; Kumar; Vasisht
Journal of the Indian Chemical Society, 1990 , vol. 67, # 12 p. 995 - 996
反应条件
1: (COCl)2 / CH2Cl2 / 3 h / Ambient temperature
2: diethyl ether / 1.) -60 deg C to 10 deg C, 2.) 10 deg C, 1 h
View Scheme
参考文献
Abarbri, Mohamed; Parrain, Jean-Luc; Duchene, Alain
Synthetic Communications, 1998 , vol. 28, # 2 p. 239 - 249
反应条件
sodium hydroxide; sodium dithionite; sodium hydrogencarbonate in water
T=90°C; 1 h; Yield given. Yields of byproduct given;
参考文献
Camps, Francisco; Coll, Jose; Guerrero, Angel; Guitart, Josefa; Riba, Magi
Chemistry Letters, 1982 , p. 715 - 718
