1,2-二己酰-Sn-甘油合成路线 （共 6 条）
反应条件
hydrogen; palladium on activated charcoal in ethanol; acetic acid Ambient temperature;
参考文献
Martin, Stephen F.; Josey, John A.; Wong, Yue-Ling; Dean, Daniel W.
Journal of Organic Chemistry, 1994 , vol. 59, # 17 p. 4805 - 4820
反应条件
1: 84 percent / Et3N, 4-(dimethylamino)pyridine / CH2Cl2 / 6 h / 25 °C 2: 85 percent / AcOH, H2 / 10percent Pd/C / propan-2-ol / 18 h / 2585.7 Torr View Scheme
参考文献
Wheeler; Blanchard; Andrews; Fang; Gray-Nunez; Harris; Lambert; Mehrotra; Parks; Ray; Smalley Jr.
Journal of Medicinal Chemistry, 1994 , vol. 37, # 24 p. 4118 - 4129
反应条件
1: 86 percent / DCC, DMAP / CH2Cl2 / 10 h / Ambient temperature 2: 87 percent / H2 / 10percent Pd/C / ethanol; acetic acid / Ambient temperature View Scheme
参考文献
Martin, Stephen F.; Josey, John A.; Wong, Yue-Ling; Dean, Daniel W.
Journal of Organic Chemistry, 1994 , vol. 59, # 17 p. 4805 - 4820
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone
参考文献
Schlueter, Urs; Lu, Jun; Fraser-Reid, Bert
Organic Letters, 2003 , vol. 5, # 3 p. 255 - 257
反应条件
oat seed lipase; water T=37°C; 0.0833333 h; pH 8.5 (Tris-HCl buffer);
参考文献
Ota, Yasuhide; Minesaki, Toshio; Oshima, Aki
Bioscience, Biotechnology and Biochemistry, 1997 , vol. 61, # 1 p. 166 - 167
反应条件
1: N,N-diisopropylethylamine / tetrahydrofuran / 0.75 h / -78 °C 2: N,N-diisopropylethylamine / tetrahydrofuran / -78 °C / -78 deg C, 2 h; r.t., 1 h 3: 30percent H2O2 / CH2Cl2 / 1 h / 0 °C 4: 83 percent / toluene / 24 h / 40 - 60 °C View Scheme
参考文献
Martin, Stephen F.; Josey, John A.; Wong, Yue-Ling; Dean, Daniel W.
Journal of Organic Chemistry, 1994 , vol. 59, # 17 p. 4805 - 4820
