1,4-二溴-2,3-双(溴甲基)-2-丁烯合成路线 （共 19 条）
反应条件
1: With bromine in tetrachloromethane T=0°C; 3 h; 2: With N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane 12 h; Heating;
参考文献
Hingston, Timothy J.; Sambrook, Mark R.; Porfyrakis, Kyriakos; Briggs, G. Andrew D.
Tetrahedron Letters, 2006 , vol. 47, # 42 p. 7413 - 7415
参考文献
Journal of Organic Chemistry, , vol. 38, p. 1367 - 1369
反应条件
hydrogen bromide; bromine T=42 - 46°C; 10 h;
参考文献
Jendralla, Heiner; Fischer, Gerd
Heterocycles, 1995 , vol. 41, # 6 p. 1291 - 1298
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane Heating;
参考文献
Tetrahedron Letters, , vol. 39, # 23 p. 4095 - 4098
反应条件
hydrogen bromide; bromine
参考文献
Chemische Berichte, , vol. 104, p. 71 - 74
反应条件
hydrogen bromide; bromine
参考文献
Chemische Berichte, , vol. 104, p. 71 - 74
反应条件
hydrogen bromide; bromine
参考文献
Chemische Berichte, , vol. 104, p. 71 - 74
反应条件
hydrogen bromide; bromine
参考文献
Chemische Berichte, , vol. 104, p. 71 - 74
反应条件
zinc in tetrahydrofuran fast addn. of concd. soln. of Ge halide and a large excess of tetrabromide to a heated suspension of activated Zn; refluxing, 2h;
参考文献
Laurent, C.; Mazerolles, P.
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1992 , vol. 22, p. 1183 - 1194
反应条件
Na or Li in tetrahydrofuran byproducts: NaCl or LiCl, NaBr or LiBr; mixt. boiled for 3-4 h; GC-MS detn. of products;
参考文献
Mazerolles, Pierre; Laurent, Christian
Journal of Organometallic Chemistry, 1992 , vol. 439, # 2 p. 115 - 125
