3,4,4-三甲基-2-环戊烯-1-酮合成路线 (共 18 条)
参考文献
Conia,J.-M.; Leriverend,M.-L.
Bulletin de la Societe Chimique de France, 1970 , p. 2981 - 2991
参考文献
Conia,J.-M.; Leriverend,M.-L.
Bulletin de la Societe Chimique de France, 1970 , p. 2981 - 2991
反应条件
1: 77 percent / H2SO4 / 0.42 h / 90 °C 2: 26 percent / NaOH / H2O / 0.5 h / Heating View Scheme
参考文献
Cadman, Michael L. F.; Crombie, Leslie; Freeman, Stephen; Mistry, Jayshree
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 11 p. 1397 - 1408
反应条件
1: 48 percent / magnesium methoxide / methanol / 24 h / Ambient temperature 2: NaOH / H2O / 2 h / Heating View Scheme
参考文献
Cadman, Michael L. F.; Crombie, Leslie; Freeman, Stephen; Mistry, Jayshree
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 11 p. 1397 - 1408
反应条件
sodium hydroxide in water 2 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Cadman, Michael L. F.; Crombie, Leslie; Freeman, Stephen; Mistry, Jayshree
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 11 p. 1397 - 1408
参考文献
Conia,J.-M.; Leriverend,M.-L.
Bulletin de la Societe Chimique de France, 1970 , p. 2992 - 2998
反应条件
Yield given. Multistep reaction;
参考文献
Greene, Andrew E.; lamsard, Jean-Philippe; Luche, Jean-Louis; Petrier, Christian
Journal of Organic Chemistry, 1984 , vol. 49, # 5 p. 931 - 932
反应条件
potassium hydroxide; sodium 1.) 0 deg C, overnight; 2.) reflux, 4 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Yates, Peter; Burke, Patrick Michael
Canadian Journal of Chemistry, 1987 , vol. 65, p. 1695 - 1704