4-苯基-2,6-二甲基吡啶合成路线 （共 24 条）
反应条件
[Re2(CO)10]; carbamic acid methyl ester in 1,4-dioxane T=135°C; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Yamamoto, Shun-Ichi; Okamoto, Kana; Murakoso, Makiko; Kuninobu, Yoichiro; Takai, Kazuhiko
Organic Letters, 2012 , vol. 14, # 12 p. 3182 - 3185
反应条件
NiCl2((PPh3)P)2 in diethyl ether; benzene T=80°C; 12 h;
参考文献
Gupta, Arun K.; Ila, Hiriyakkanavar; Junjappa, Hiriyakkanavar
Tetrahedron, 1990 , vol. 46, # 7 p. 2561 - 2572
反应条件
[Re2(CO)10] in toluene T=180°C; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Yamamoto, Shun-Ichi; Okamoto, Kana; Murakoso, Makiko; Kuninobu, Yoichiro; Takai, Kazuhiko
Organic Letters, 2012 , vol. 14, # 12 p. 3182 - 3185
反应条件
kaolin; ammonia; acetone T=310°C;
参考文献
Frank; Seven
Journal of the American Chemical Society, 1949 , vol. 71, p. 2629,2633
反应条件
ammonium acetate; ammonia; water T=250°C;
参考文献
Frank; Meikle
Journal of the American Chemical Society, 1950 , vol. 72, p. 4184
反应条件
ammonia; cadmium calcium phosphate T=350 - 400°C; flow-type reactor;
参考文献
Soldatenkov, A. T.; Fedorov, V. O.; Chandra, R.; Polosin, V. M.; Mikaya, A. I.; Prostakov, N. S.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 179 - 185
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 1 p. 188 - 194
反应条件
hydrogen; nickel in methanol 24 h;
参考文献
Batra, Sanjay; Seth, M; Bhaduri, A P
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 1 p. 60 - 62
反应条件
oxygen; copper(II) bis(trifluoromethanesulfonate) T=100°C; 20 h; Sealed tube;
参考文献
Huang, Huawen; Ji, Xiaochen; Wu, Wanqing; Huang, Liangbin; Jiang, Huanfeng
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 3774 - 3782
反应条件
zinc; tetrakis(triphenylphosphine) palladium(0) 1) THF, r.t., 5 h, 2) r.t., 51 h; Yield given. Multistep reaction;
参考文献
Sakamoto, Takao; Kondo, Yoshinori; Murata, Naoko; Yamanaka, Hiroshi
Tetrahedron, 1993 , vol. 49, # 43 p. 9713 - 9720
反应条件
1: orthophosphoric acid / 3 h / 130 °C 2: 85 percent / <(C6H5)3P>2NiCl2 / benzene; diethyl ether / 12 h / 80 °C View Scheme
参考文献
Gupta, Arun K.; Ila, Hiriyakkanavar; Junjappa, Hiriyakkanavar
Tetrahedron, 1990 , vol. 46, # 7 p. 2561 - 2572
