7-氨基-1-甲基-1,2,3,4-四氢喹啉合成路线 （共 6 条）
反应条件
hydrogen; palladium on activated charcoal in methanol T=20°C; P=760 Torr;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 16, # 17 p. 4533 - 4536
反应条件
1: 63 percent / HNO3; H2SO4 / 0 - 5 °C 2: K2CO3 / dimethylformamide / 20 °C 3: H2 / Pd/C / methanol / 20 °C / 760 Torr View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 16, # 17 p. 4533 - 4536
反应条件
1: K2CO3 / dimethylformamide / 20 °C 2: H2 / Pd/C / methanol / 20 °C / 760 Torr View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 16, # 17 p. 4533 - 4536
反应条件
1: in toluene T=10 - 20°C; 2: With water in toluene T=10 - 25°C; 1 h;
参考文献
MITSUBISHI CHEMICAL CORPORATION; Mitsubishi Kagaku Media Co., Ltd.
Patent: EP1666538 A1, 2006 ;
Location in patent: Page/Page column 73-75 ;
反应条件
phosphoric acid in water
24 h; Reflux;
参考文献
MICHIGAN TECHNOLOGICAL UNIVERSITY; BI, Lanrong
Patent: WO2014/63033 A2, 2014 ;
Location in patent: Paragraph 00181 ;
反应条件
1: in toluene
T=10 - 20°C;
2: With water in toluene
T=10 - 25°C; 1 h;
参考文献
MITSUBISHI CHEMICAL CORPORATION; Mitsubishi Kagaku Media Co., Ltd.
Patent: EP1666538 A1, 2006 ;
Location in patent: Page/Page column 73-75 ;
