3-乙基-3-氧杂丁环甲醇合成路线 （共 17 条）
反应条件
Jone's reagent in acetone T=-5 - 25°C; 6 h;
参考文献
Journal of Polymer Science, Part A: Polymer Chemistry, , vol. 50, # 3 p. 458 - 465
反应条件
hydrogenchloride in tetrahydrofuran; water T=0 - 20°C;
参考文献
Mindemark, Jonas; Bowden, Tim
Polymer, 2011 , vol. 52, # 25 p. 5716 - 5722
反应条件
sodium hydroxide; tetrabutylammomium bromide in hexane; water 5 h; Heating / reflux;
参考文献
MERCK PATENT GMBH
Patent: WO2005/121150 A1, 2005 ;
Location in patent: Page/Page column 48 ;
反应条件
hydrogen bromide in tetrahydrofuran; water T=25°C; 5 h;
参考文献
SSENS B.V.
Patent: WO2013/4296 A1, 2013 ;
Location in patent: Page/Page column 18 ;
反应条件
oxalyl dichloride; dimethyl sulfoxide; triethylamine
1.) CH2Cl2, 2.) CH2Cl2; Multistep reaction;
参考文献
Smith, Ian H.; Budd, Timothy C.; Sills, Jill; Casida, John E.
Journal of Agricultural and Food Chemistry, 1993 , vol. 41, # 7 p. 1114 - 1117
参考文献
Singha, Nikhil K.; De Ruiter, Barteld; Schubert, Ulrich S.
Macromolecules, 2005 , vol. 38, # 9 p. 3596 - 3600
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
T=0 - 10°C; 24 h;
参考文献
National Starch and Chemical Investment Holding Corporation
Patent: EP1621534 A2, 2006 ;
Location in patent: Page/Page column 6 ;
