苄基-(5,6-二氢-4H-[1,3]噻嗪-2-基)-胺合成路线 （共 8 条）
反应条件
hydrogenchloride; sodium carbonate 24 h; Heating;
参考文献
Caujolle, Raymond; Amarouch, Hamid; Payard, Marc; Loiseau, Philippe R.; Bories, Christian; et al.
European Journal of Medicinal Chemistry, 1989 , vol. 24, p. 287 - 292
反应条件
methanol anschliessend Behandeln mit einem Ionenaustauscher;
参考文献
McKay et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 3335,3338
反应条件
1: 3 N HCl, triethylamine / CHCl3 2: acetone / 5 h / Heating 3: 58 percent / 1.) 6 N HCl; 2.) 10 percent Na2CO3, pH=10-11 / 24 h / Heating View Scheme
参考文献
Caujolle, Raymond; Amarouch, Hamid; Payard, Marc; Loiseau, Philippe R.; Bories, Christian; et al.
European Journal of Medicinal Chemistry, 1989 , vol. 24, p. 287 - 292
反应条件
1: acetone / 5 h / Heating 2: 58 percent / 1.) 6 N HCl; 2.) 10 percent Na2CO3, pH=10-11 / 24 h / Heating View Scheme
参考文献
Caujolle, Raymond; Amarouch, Hamid; Payard, Marc; Loiseau, Philippe R.; Bories, Christian; et al.
European Journal of Medicinal Chemistry, 1989 , vol. 24, p. 287 - 292
反应条件
1: triethylamine / CHCl3 / 1 h / Ambient temperature 2: 3 N HCl, triethylamine / CHCl3 3: acetone / 5 h / Heating 4: 58 percent / 1.) 6 N HCl; 2.) 10 percent Na2CO3, pH=10-11 / 24 h / Heating View Scheme
参考文献
Caujolle, Raymond; Amarouch, Hamid; Payard, Marc; Loiseau, Philippe R.; Bories, Christian; et al.
European Journal of Medicinal Chemistry, 1989 , vol. 24, p. 287 - 292
反应条件
1: benzene / 8 h / 0 °C 2: triethylamine / CHCl3 / 1 h / Ambient temperature 3: 3 N HCl, triethylamine / CHCl3 4: acetone / 5 h / Heating 5: 58 percent / 1.) 6 N HCl; 2.) 10 percent Na2CO3, pH=10-11 / 24 h / Heating View Scheme
参考文献
Caujolle, Raymond; Amarouch, Hamid; Payard, Marc; Loiseau, Philippe R.; Bories, Christian; et al.
European Journal of Medicinal Chemistry, 1989 , vol. 24, p. 287 - 292
反应条件
lithium aluminium tetrahydride
参考文献
Schoeberl,A.; Magosch,K.-H.
Justus Liebigs Annalen der Chemie, 1970 , vol. 742, p. 74 - 84
反应条件
(i) NaOEt, EtOH, (ii) /BRN= 386135/; Multistep reaction;
参考文献
Schoeberl,A.; Magosch,K.-H.
Justus Liebigs Annalen der Chemie, 1970 , vol. 742, p. 74 - 84
