acetic anhydride; p-nitrosobenzene in benzene at room temp. stirring mixt. for 1 h under Ar in the dark, addn. of acetic anhydride, addn. of mixt. to iron powder in AcOH, stirring for 4 h at 100°C; filtn. washing ppt. with ether, neutralising org. phase with aq. NaOH, washing with brine, drying, distn., t.l.c.;
参考文献
Barton, Derek H. R.; Finet, Jean-Pierre; Giannotti, Charles; Halley, Frank
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 241 - 250
Barton, Derek H. R.; Blazejewski, Jean-Claude; Charpiot, Brigitte; Motherwell, William B.
Journal of the Chemical Society, Chemical Communications, 1981 , # 10 p. 503 - 504
acetic anhydride; p-nitrosobenzene in benzene at room temp. stirring mixt. for 1 h under Ar in the dark, addn. of acetic anhydride, addn. of mixt. to iron powder in AcOH, stirring for 4 h at 100°C; filtn. washing ppt. with ether, neutralising org. phase with aq. NaOH, washing with brine, drying, distn., t.l.c.;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 241 - 250
Barton, Derek H. R.; Blazejewski, Jean-Claude; Charpiot, Brigitte; Lester, David J.; Motherwell, William B.; Papoula, M. Teresa Barros
Journal of the Chemical Society, Chemical Communications, 1980 , # 17 p. 827 - 829
in toluene 0.5 h, 20°C; solvent and bromobenzene removing, crystals washing (petroleum ether) and drying, Ph4SbBr in residue, Ph3Bi in petroleum ether soln.;
参考文献
Russian Journal of General Chemistry, , vol. 68, p. 318 - 319
Zhurnal Obshchei Khimii, , vol. 68, p. 345 - 346
