2,6-二碘-4-硝基苯酚合成路线 (共 29 条)
参考文献
Jahresbericht ueber die Fortschritte der Chemie und Verwandter Theile Anderer Wissenschaften, , p. 616
Zeitschrift fuer Chemie, , p. 324
参考文献
Chemische Berichte, , vol. 70, p. 146,149, 150
参考文献
Justus Liebigs Annalen der Chemie, , vol. 174, p. 100
反应条件
potassium carbonate in acetone T=65°C; 18 h; Inert atmosphere;
参考文献
Beale, Thomas M.; Allwood, Daniel M.; Bender, Andreas; Bond, Peter J.; Brenton, James D.; Charnock-Jones, D. Stephen; Ley, Steven V.; Myers, Rebecca M.; Shearman, James W.; Temple, Jill; Unger, Jessica; Watts, Ciorsdaidh A.; Xian, Jian
ACS Medicinal Chemistry Letters, 2012 , vol. 3, # 3 p. 177 - 181
反应条件
potassium carbonate in N,N-dimethyl-formamide T=70°C; 60 h;
参考文献
Helgeson, Roger C.; Czech, Bronislaw P.; Chapoteau, Eddy; Gebauer, Carl R.; Kumar, Anand; Cram, Donald J.
Journal of the American Chemical Society, 1989 , vol. 111, # 16 p. 6339 - 6350
反应条件
hydrogenchloride; tin(ll) chloride
参考文献
Block; Powell
Journal of the American Chemical Society, 1942 , vol. 64, p. 1070,1072
反应条件
sodium hydroxide; sodium dithionite T=75°C;
参考文献
Kunz; Iyengar; Dorr; Alberts; Remers
Journal of Medicinal Chemistry, 1991 , vol. 34, # 7 p. 2281 - 2286
反应条件
tin; acetic acid
anschliessendes Behandeln mit CrO3 in wss. H2SO4;
参考文献
Woollett et al.
Journal of the American Chemical Society, 1937 , vol. 59, p. 861,862
反应条件
1: sodium dithionite; aqueous sodium carbonate
2: ethanolic H2SO4 / Diazotization.anschliessendes Kochen
View Scheme
参考文献
Woollett et al.
Journal of the American Chemical Society, 1937 , vol. 59, p. 861,862