(1-甲基-1H-2-咪唑基)(苯基)甲醇合成路线 (共 6 条)
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran; hexane T=-78°C; 1 h;
参考文献
Miyashita, Akira; Kurachi, Akihito; Matsuoka, Yoshiyuki; Tanabe, Noriko; Suzuki, Yumiko; Iwamoto, Ken-Ichi; Higashino, Takeo
Heterocycles, 1997 , vol. 44, # 1 p. 417 - 426
反应条件
water; trifluoroacetic acid in tetrahydrofuran Heating; Product distribution; Further Variations:Reaction partnersReagentsSolvents;
参考文献
Deng, Yijun; Hlasta, Dennis J.
Tetrahedron Letters, 2002 , vol. 43, # 2 p. 189 - 192
反应条件
in diethyl ether T=20°C;
参考文献
Abarca-Gonzalez, Belen; Jones, R. Alan; Medio-Simon, Mercedes; Quilez-Pardo, Juan; Sepulveda-Arques, Jose; Zaballos-Garcia, Elena
Synthetic Communications, 1990 , vol. 20, # 3 p. 321 - 331
反应条件
sodium acetate; pyridinium chlorochromate in dichloromethane T=20°C; 2 h; Yield given;
参考文献
Abarca-Gonzalez, Belen; Jones, R. Alan; Medio-Simon, Mercedes; Quilez-Pardo, Juan; Sepulveda-Arques, Jose; Zaballos-Garcia, Elena
Synthetic Communications, 1990 , vol. 20, # 3 p. 321 - 331
反应条件
1: 85 percent / dimethylformamide / 3 h / Heating
2: 57 percent / NaH / tetrahydrofuran / 1 h / Heating
View Scheme
参考文献
Miyashita, Akira; Kurachi, Akihito; Matsuoka, Yoshiyuki; Tanabe, Noriko; Suzuki, Yumiko; Iwamoto, Ken-Ichi; Higashino, Takeo
Heterocycles, 1997 , vol. 44, # 1 p. 417 - 426
反应条件
1: 85 percent / dimethylformamide / 3 h / Heating
2: 62 percent / NaH / tetrahydrofuran / 1 h / Heating
View Scheme
参考文献
Miyashita, Akira; Kurachi, Akihito; Matsuoka, Yoshiyuki; Tanabe, Noriko; Suzuki, Yumiko; Iwamoto, Ken-Ichi; Higashino, Takeo
Heterocycles, 1997 , vol. 44, # 1 p. 417 - 426