(6CI,8CI,9CI)-4-乙基嘧啶合成路线 （共 8 条）
反应条件
hydrogen; sodium acetate; palladium on activated charcoal in methanol; ethanol T=50°C; P=2585.7 Torr; 3 h;
参考文献
Butters, M.
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 5 p. 1369 - 1370
反应条件
1: 85 percent / phosphorus oxychloride / CH2Cl2 / 3 h / Heating 2: 73 percent / H2, sodium acetate, / 5percent Pd/C / ethanol; methanol / 3 h / 50 °C / 2585.7 Torr View Scheme
参考文献
Butters, M.
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 5 p. 1369 - 1370
反应条件
1: 67 percent / sodium methoxide / methanol / 4 h / Ambient temperature 2: 85 percent / phosphorus oxychloride / CH2Cl2 / 3 h / Heating 3: 73 percent / H2, sodium acetate, / 5percent Pd/C / ethanol; methanol / 3 h / 50 °C / 2585.7 Torr View Scheme
参考文献
Butters, M.
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 5 p. 1369 - 1370
反应条件
palladium on activated charcoal; ethanol Hydrogenation;
参考文献
Overberger; Kogon
Journal of the American Chemical Society, 1954 , vol. 76, p. 1879,1882
反应条件
1: 165 °C 2: KOH / unter vermindertem Druck 3: palladium/charcoal; ethanol / Hydrogenation View Scheme
参考文献
Overberger; Kogon
Journal of the American Chemical Society, 1954 , vol. 76, p. 1879,1882
反应条件
1: palladium/charcoal; MgO; aqueous ethanol / Hydrogenation 2: 165 °C 3: KOH / unter vermindertem Druck 4: palladium/charcoal; ethanol / Hydrogenation View Scheme
参考文献
Overberger; Kogon
Journal of the American Chemical Society, 1954 , vol. 76, p. 1879,1882
反应条件
1: KOH / unter vermindertem Druck 2: palladium/charcoal; ethanol / Hydrogenation View Scheme
参考文献
Overberger; Kogon
Journal of the American Chemical Society, 1954 , vol. 76, p. 1879,1882
参考文献
Bredereck et al.
Chemische Berichte, 1957 , vol. 90, p. 942,951
Chemische Berichte, 1958 , vol. 91, p. 2830,2831
