N-[3-(4,4,5,5-四甲基-1,3,2-二氧杂硼烷-2-基)苯基]甲基磺酰氯合成路线 （共 4 条）
反应条件
1: in ethylene glycol dimethyl ether 0.166667 h; Inert atmosphere; 2: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate in ethylene glycol dimethyl ether T=80°C; Inert atmosphere;
参考文献
AURIGENE DISCOVERY TECHNOLOGIES LIMITED; UM PHARMAUJI SDN. BHD; GUMMADI, Venkateshwar, Rao; HOSAHALLI, Subramanya; NANDURI, Srinivas; AGGUNDA RENUKAPPA, Girish
Patent: WO2014/6554 A1, 2014 ;
Location in patent: Page/Page column 28 ;
参考文献
Kressierer, Christoph J.; Lehnemann, Bernd; Jung, Jorg
Patent: US2008/269523 A1, 2008 ;
Location in patent: Page/Page column 6 ;
反应条件
in DMF (N,N-dimethyl-formamide) T=50°C; 44 h;
参考文献
Davison, Joshua Zwick; Jones, Winton Dennis; Zarrinmayeh, Hamideh; Zimmerman, Dennis Michael
Patent: US2003/225266 A1, 2003 ;
Location in patent: Page 24 ;
反应条件
1.1: pyridine / dichloromethane / 15 h / 10 - 20 °C 2.1: ethylene glycol dimethyl ether / 0.17 h / |Inert atmosphere 2.2: 80 °C / |Inert atmosphere View Scheme
