反应条件
1: 1) LiAlH4 / 1) THF, warm to RT, 0.25 h, 2) reflux, 2 h 2: 85 percent / glacial acetic acid / H2O / 1 h / 80 - 90 °C 3: 99 percent / glacial acetic acid, H2O2 / tetrahydrofuran / 1) 0 deg C, 0.25 h, 2) warm to RT, 1 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 56, # 6 p. 2161 - 2165
