ETHYL 5-硝基-2-吡啶乙基甲苯合成路线 （共 6 条）
反应条件
Dowex 50W in benzene
参考文献
Schneider; Harris
Journal of Organic Chemistry, 1984 , vol. 49, # 20 p. 3681 - 3684
反应条件
1: 83 percent / chromium trioxide/conc. H2SO4 / Ambient temperature 2: 97 percent / Dowex 50W / benzene View Scheme
参考文献
Schneider; Harris
Journal of Organic Chemistry, 1984 , vol. 49, # 20 p. 3681 - 3684
反应条件
1: 55 percent 2: 83 percent / chromium trioxide/conc. H2SO4 / Ambient temperature 3: 97 percent / Dowex 50W / benzene View Scheme
参考文献
Schneider; Harris
Journal of Organic Chemistry, 1984 , vol. 49, # 20 p. 3681 - 3684
反应条件
diisobutylaluminium hydride; Sodium potassium tartrate in dichloromethane; water T=-78 - 20°C; Inert atmosphere;
参考文献
NOVARTIS AG
Patent: WO2009/141386 A1, 2009 ;
Location in patent: Page/Page column 88 ;
WO 2009/141386 A1
反应条件
diisobutylaluminium hydride in dichloromethane T=-78 - 20°C;
参考文献
NOVARTIS AG
Patent: WO2009/141386 A1, 2009 ;
Location in patent: Page/Page column 136 ;
WO 2009/141386 A1
反应条件
hydrogen; palladium 10 on activated carbon in ethanol P=2068.65 Torr; 4 h;
参考文献
PFIZER INC.
Patent: WO2004/14904 A1, 2004 ;
Location in patent: Page 54 ;
WO 2004/014904 A1
