1-苄基-3-碘哌啶-2-酮合成路线 (共 4 条)
反应条件
sodium iodide in acetone Substitution; 17 h; Heating;
参考文献
Dyer, James; King, Amanda; Keeling, Steve; Moloney, Mark G.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 16 p. 2793 - 2804
反应条件
1.1: NaH / tetrahydrofuran / 0.5 h / 0 °C 1.2: 85 percent / tetrahydrofuran / 21 h 2.1: sec-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C 2.2: 71 percent / p-TsCl / tetrahydrofuran; hexane / 16 h / 20 °C 3.1: 90 percent / NaI / acetone / 17 h / Heating View Scheme
参考文献
Dyer, James; King, Amanda; Keeling, Steve; Moloney, Mark G.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 16 p. 2793 - 2804
反应条件
1.1: sec-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C 1.2: 71 percent / p-TsCl / tetrahydrofuran; hexane / 16 h / 20 °C 2.1: 90 percent / NaI / acetone / 17 h / Heating View Scheme
参考文献
Dyer, James; King, Amanda; Keeling, Steve; Moloney, Mark G.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 16 p. 2793 - 2804
反应条件
1.1: NaH / tetrahydrofuran / 0.5 h / 0 °C 1.2: 85 percent / tetrahydrofuran / 21 h 2.1: sec-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C 2.2: 71 percent / p-TsCl / tetrahydrofuran; hexane / 16 h / 20 °C 3.1: 90 percent / NaI / acetone / 17 h / Heating View Scheme
参考文献
Dyer, James; King, Amanda; Keeling, Steve; Moloney, Mark G.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 16 p. 2793 - 2804