2,2-二氯-1,1,1-三氟乙烷合成路线 (共 115 条)
反应条件
sulfur(IV) fluoride T=80 - 90°C; 3 h;
参考文献
Wielgat,J.; Domagala,Z.
Journal of Fluorine Chemistry, 1982 , vol. 20, p. 785
反应条件
hydrogenchloride; aluminium trichloride T=180°C; 23 h;
参考文献
Tetrahedron, , vol. 18, p. 123 - 133
反应条件
sodium hypochlorite in acetonitrile T=-10 - 10°C; 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 28, # 1.1 p. 20 - 28
Zhurnal Organicheskoi Khimii, , vol. 28, # 1 p. 25 - 35
反应条件
sulfur(IV) fluoride T=50 - 60°C; 3 h;
参考文献
Journal of Fluorine Chemistry, , vol. 20, p. 785
反应条件
an activated AlF3 T=210 - 240°C; 0.00972222 h; Gas phasea fluid-bed reactor; Product distribution / selectivity;
参考文献
EP1502906 A1, ;
Page 7-8 ;
反应条件
1: With hydrogen fluoride; chromium-based fluorination catalyst 2: With Cr on active alumina catalyst T=180°C; 4 h; Inconel 600 type reactor; Product distribution / selectivity;
参考文献
WO2005/92823 A2, ;
Page/Page column 11; 16 ;
参考文献
Industrial and Engineering Chemistry, , vol. 39, p. 412,413
反应条件
hydrogen fluoride; antimony(V) pentachloride; chlorine T=160°C;
参考文献
Gazzetta Chimica Italiana, , vol. 89, p. 1608,1614
反应条件
hydrogen fluoride; antimony(V) pentachloride; chlorine T=125°C;
参考文献
Gazzetta Chimica Italiana, , vol. 89, p. 1608,1614
反应条件
sulfur(IV) fluoride T=60°C; 3 h;
参考文献
Roczniki Chemii, , vol. 47, p. 1211 - 1221