2,2-二氯-1,1,1-三氟乙烷合成路线 (共 115 条)
反应条件
nitric oxide in neat (no solvent) T=23°C; P=1.2 - 23.8 Torr; Irradiation; Quantum yieldRate constantMechanism;
参考文献
Yano, T.; Jung, K.-H.; Tschuikow-Roux, E.
Journal of Physical Chemistry, 1980 , vol. 84, # 17 p. 2146 - 2151
反应条件
1: With hydrogen fluoride 2: With hydrogen T=220°C; P=1125.11 Torr; In the presence of catalyst;
参考文献
SHOWA DENKO K. K.
Patent: WO2004/5226 A1, 2004 ;
Location in patent: Page 12-13 ;
反应条件
[2,2']bipyridinyl; copper(I) chloride; copper in N,N-dimethyl-formamide T=20 - 80°C; P=992.774 - 1303.07 Torr; Inert atmosphere; Product distribution / selectivity;
参考文献
WO2009/117458 A2, ;
Page/Page column 4-5 ;
反应条件
diethylamine; copper T=20°C; P=915.2 - 1018.63 Torr; 64 h; Inert atmosphere; Product distribution / selectivity;
参考文献
WO2009/117458 A2, ;
Page/Page column 8-9 ;
反应条件
copper(I) chloride; copper T=20 - 80°C; P=966.916 - 1328.93 Torr; Inert atmosphere; Product distribution / selectivity;
参考文献
WO2009/117458 A2, ;
Page/Page column 7-8 ;
反应条件
1: With hydrogen fluoride 2: With hydrogen T=220°C; P=1125.11 Torr; In the presence of catalyst;
参考文献
SHOWA DENKO K. K.
Patent: WO2004/5226 A1, 2004 ;
Location in patent: Page 12-13 ;
反应条件
hydrogen fluoride; fluorinated chromium oxide T=320°C; P=2353.83 Torr; 60 h;
参考文献
Daikin Industries, Ltd.
Patent: US6392106 B1, 2002 ;
Location in patent: Page column 5-7 ;
反应条件
1: With hydrogen fluoride 2: With hydrogen T=220°C; P=1125.11 Torr; In the presence of catalyst;
参考文献
SHOWA DENKO K. K.
Patent: WO2004/5226 A1, 2004 ;
Location in patent: Page 12-13 ;
反应条件
nitrogen trifluoride; hydrogen fluoride; oxygen; chromium based-catalyst Further byproducts. Title compound not separated from byproducts.;
参考文献
Belter, Randolph K.; Sweval, Mark S.; Iikubo, Yuichi
Journal of Fluorine Chemistry, 2006 , vol. 127, # 6 p. 816 - 820
反应条件
1: With hydrogen fluoride 2: With hydrogen T=220°C; P=1125.11 Torr; In the presence of catalyst;
参考文献
SHOWA DENKO K. K.
Patent: WO2004/5226 A1, 2004 ;
Location in patent: Page 12-13 ;