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hydrogenchloride; sodium hydroxide in tetrahydrofuran; water NaN3 was added to a THF soln. of trialkylborane followed by 10percent aq. HCl, mixt. was gently relfuxed overnight; dild. with aq. HCl, extd. with ether, aq. layer was made basic (aq. NaOH) and ext. with ether, ether exts. were dried over KOH, filtered, evapd.;