4-(4-二甲基氨基苯基)丁-3-烯-2-酮合成路线 (共 4 条)
反应条件
sodium hydroxide in water T=5 - 10°C; 0.583333 h;
参考文献
Paul, Satya; Gupta, Monika
Synthetic Communications, 2005 , vol. 35, # 2 p. 213 - 222
反应条件
caesium carbonate in 1,4-dioxane; water T=20°C; 16 h; Inert atmosphere;
参考文献
Lalonde, Mathieu P.; McGowan, Meredeth A.; Rajapaksa, Naomi S.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2013 , vol. 135, # 5 p. 1891 - 1894
反应条件
palladium diacetate; copper (II) acetate monohydrate; potassium carbonate in N,N-dimethyl-formamide T=120°C; Inert atmosphere;
参考文献
Unoh, Yuto; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Journal of Organic Chemistry, 2013 , vol. 78, # 10 p. 5096 - 5102
反应条件
in dichloromethane T=50°C; P=10000 Torr; 4 h;
参考文献
Nonnenmacher, Axel; Mayer, Richard; Plieninger, Hans
Liebigs Annalen der Chemie, 1983 , # 12 p. 2135 - 2140