1-(4-吗啉基)-1-丙酮合成路线 (共 12 条)
反应条件
pyridine in dichloromethane T=0 - 20°C; 2 h;
参考文献
Hama, Takuo; Culkin, Darcy A.; Hartwig, John F.
Journal of the American Chemical Society, 2006 , vol. 128, # 15 p. 4976 - 4985
反应条件
triethylamine in dichloromethane T=0 - 20°C; 3.5 h;
参考文献
Peters, Rene; Diolez, Christian; Rolland, Alain; Manginot, Eric; Veyrat, Marc
Heterocycles, 2007 , vol. 72, p. 255 - 273
反应条件
[Ru(II)(η6-benzene)(μ-Cl)Cl]2; N,N-diisopropylimidazolium bromide; sodium hydride in toluene; acetonitrile 24 h; Inert atmosphereReflux;
参考文献
Chen, Cheng; Hong, Soon Hyeok
Organic Letters, 2012 , vol. 14, # 12 p. 2992 - 2995
反应条件
in tetrahydrofuran T=20°C; 0.333333 h;
参考文献
Lemoucheux; Rouden; Lasne
Tetrahedron Letters, 2000 , vol. 41, # 51 p. 9997 - 10001
反应条件
triethylamine in dichloromethane T=20°C; 16 h;
参考文献
Grzyb, Justyna A.; Batey, Robert A.
Tetrahedron Letters, 2008 , vol. 49, # 36 p. 5279 - 5282
反应条件
hydrazine hydrate 5 h; Heating;
参考文献
Basanagouda, Mahantesha; Kulkarni, Manohar V.; Kalkhambkar, Raj G.; Kulkarni, Geeta M.
Synthetic Communications, 2008 , vol. 38, # 17 p. 2929 - 2940
反应条件
Iron (III) nitrate nonahydrate T=125°C; 24 h; Neat (no solvent)Sealed tube;
参考文献
Allen, C. Liana; Lapkin, Alexei A.; Williams, Jonathan M.J.
Tetrahedron Letters, 2009 , vol. 50, # 29 p. 4262 - 4264
反应条件
1: 0.08 h / Heating 2: 38 percent / tetrahydrofuran / 0.33 h / 20 °C View Scheme
参考文献
Lemoucheux; Rouden; Lasne
Tetrahedron Letters, 2000 , vol. 41, # 51 p. 9997 - 10001
反应条件
trichlorophosphate in 1,2-dichloro-ethane Vilsmeier-Haack reaction;
参考文献
Loussouarn; Servant; Guervenou; Sturtz
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 113, # 1-4 p. 275 - 285
反应条件
dimethyl sulfate 120 h, heating, ether; Yield given. Multistep reaction;
参考文献
Kantlehner, Willi; Gutbrod, Heinz-Dieter
Liebigs Annalen der Chemie, 1980 , # 11 p. 1677 - 1688