苯并[b]芘-1,6-二酮合成路线 (共 38 条)
反应条件
manganese triacetate in acetic acid T=40°C; 0.5 h; Title compound not separated from byproducts;
参考文献
Cremonesi, Paolo; Cavalieri, Ercole L.; Rogan, Eleanor G.
Journal of Organic Chemistry, 1989 , vol. 54, # 15 p. 3561 - 3570
反应条件
n-Pentyl nitrite; sulfuric acid; acetic acid T=0 - 5°C; anschliessend Erwaermen mit wss. Schwefelsaeure;
参考文献
Fieser; Hershberg
Journal of the American Chemical Society, 1939 , vol. 61, p. 1565,1571
反应条件
n-Pentyl nitrite; sulfuric acid; acetic acid T=0 - 5°C; anschliessend Erwaermen mit wss. Schwefelsaeure;
参考文献
Fieser; Hershberg
Journal of the American Chemical Society, 1939 , vol. 61, p. 1565,1571
反应条件
manganese triacetate in acetic acid T=40°C; 0.416667 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Cremonesi, Paolo; Cavalieri, Ercole L.; Rogan, Eleanor G.
Journal of Organic Chemistry, 1989 , vol. 54, # 15 p. 3561 - 3570
反应条件
in acetic acid T=40°C; 0.416667 h; Further byproducts given. Yields of byproduct given;
参考文献
Cremonesi, Paolo; Cavalieri, Ercole L.; Rogan, Eleanor G.
Journal of Organic Chemistry, 1989 , vol. 54, # 15 p. 3561 - 3570
反应条件
1: diethyl ether 2: aqueous sulfuric acid; acetic acid; pentyl nitrite / 0 - 5 °C / anschliessend Erwaermen mit wss. Schwefelsaeure View Scheme
参考文献
Fieser; Hershberg
Journal of the American Chemical Society, 1939 , vol. 61, p. 1565,1571
反应条件
1,3,6,8-tetra-n-butylpyrimidolt;5,4-ggt;pteridine-2,4,5,7(1H,3H,6H,8H)-tetrone 10-oxide in acetonitrile 0.666667 h; Irradiation; Yield given;
参考文献
Lee-Ruff, E.; Kazarians-Moghaddam, H.; Katz, M.
Canadian Journal of Chemistry, 1986 , vol. 64, p. 1297 - 1303
反应条件
CAS; sulfuric acid in acetonitrile 5 h; Ambient temperature;
参考文献
Balanikas, George; Hussain, Nalband; Amin, Shantu; Hecht, Stephen S.
Journal of Organic Chemistry, 1988 , vol. 53, # 5 p. 1007 - 1010
反应条件
in acetic acid T=40°C; 0.166667 h; other 6-, 1,6-, and 3,6-substituted benzo<a>pyrenes; Product distributionMechanism;
参考文献
Cremonesi, Paolo; Cavalieri, Ercole L.; Rogan, Eleanor G.
Journal of Organic Chemistry, 1989 , vol. 54, # 15 p. 3561 - 3570
反应条件
in acetic acid T=40°C; 0.5 h; Title compound not separated from byproducts;
参考文献
Cremonesi, Paolo; Cavalieri, Ercole L.; Rogan, Eleanor G.
Journal of Organic Chemistry, 1989 , vol. 54, # 15 p. 3561 - 3570