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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
30673-29-1
合成路线
（共 12 条）
82238-23-1
→
反应条件
30673-29-1
反应条件
sodium tetrahydroborate in ethanol; dichloromethane 0.5 h; Ambient temperature;
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
88048-85-5
→
反应条件
30673-29-1
+
88048-86-6
反应条件
sulfuric acid T=95°C; 0.5 h;
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
917-64-6
magnesium,carbanide,iodide
+
82238-23-1
→
反应条件
30673-29-1
+
30571-15-4
反应条件
in diethyl ether; benzene 3 h; Heating;
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
82238-25-3
→
反应条件
30673-29-1
反应条件
1: acetonitrile / 3 h / Ambient temperature 2: 83.8 percent / diethyl ether; benzene / 3 h / Heating View Scheme
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
23974-72-3
→
反应条件
30673-29-1
反应条件
1: 86.1 percent / dimethylformamide / 4 h / 120 °C 2: 98.7 percent / diethyl ether / 1 h / Heating 3: 79.6 percent / 80percent H2SO4 / 0.5 h / 95 °C View Scheme
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
89-98-5
2-氯苯甲醛
→
反应条件
30673-29-1
反应条件
1: 86.1 percent / dimethylformamide / 4 h / 120 °C 2: 98.7 percent / diethyl ether / 1 h / Heating 3: 79.6 percent / 80percent H2SO4 / 0.5 h / 95 °C View Scheme
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
88048-84-4
→
反应条件
30673-29-1
反应条件
1: 98.7 percent / diethyl ether / 1 h / Heating 2: 79.6 percent / 80percent H2SO4 / 0.5 h / 95 °C View Scheme
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
13139-86-1
3-甲基-CBS-氧硼啶
→
反应条件
30673-29-1
+
41959-23-3
反应条件
in diethyl ether; benzene 3 h; Heating;
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
82238-23-1
+
13139-86-1
3-甲基-CBS-氧硼啶
→
反应条件
30673-29-1
+
41959-23-3
反应条件
in diethyl ether; benzene 3 h; Heating;
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
30673-29-1
→
反应条件
82238-29-7
反应条件
1: acetonitrile / 3 h / Ambient temperature; 1 eq. chloramine-B 2: acetonitrile / 3 h / Ambient temperature 3: 98 percent / toluene / 6 h / Heating View Scheme
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
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