2,3,4-三-O-乙酰基-α-D-木吡喃糖苷溴合成路线 （共 37 条）
反应条件
copper(II) sulfate; acetic acid; zinc T=-8°C;
参考文献
Helferich; Gindy
Chemische Berichte, 1954 , vol. 87, p. 1488,1490
Full Text Show Details
Brimacombe et al.
Tetrahedron, 1958 , vol. 4, p. 351,358
反应条件
1: octanol With sodium tetrahydroborate; cyanocobalamin 0.5 h; 2: 2,3,4-tri-O-acetyl-α-D-xylopyranosyl bromide T=20°C; 20 h;
参考文献
Petrovic, Zorica D.; Andjelkovic, Dejan; Spasojevic, Aleksandra
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 1 p. 272 - 275
反应条件
1: methyl butylhexanol With sodium tetrahydroborate; cyanocobalamin 0.5 h; 2: 2,3,4-tri-O-acetyl-α-D-xylopyranosyl bromide T=20°C; 20 h;
参考文献
Petrovic, Zorica D.; Andjelkovic, Dejan; Spasojevic, Aleksandra
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 1 p. 272 - 275
反应条件
1: 2-ethyl-n-hexanol With sodium tetrahydroborate; cyanocobalamin 0.5 h; 2: 2,3,4-tri-O-acetyl-α-D-xylopyranosyl bromide T=20°C; 20 h;
参考文献
Petrovic, Zorica D.; Andjelkovic, Dejan; Spasojevic, Aleksandra
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 1 p. 272 - 275
反应条件
1: heptan-1-ol With sodium tetrahydroborate; cyanocobalamin 0.5 h; 2: 2,3,4-tri-O-acetyl-α-D-xylopyranosyl bromide T=20°C; 20 h;
参考文献
Petrovic, Zorica D.; Andjelkovic, Dejan; Spasojevic, Aleksandra
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 1 p. 272 - 275
反应条件
1: decyl alcohol With sodium tetrahydroborate; cyanocobalamin 0.5 h; 2: 2,3,4-tri-O-acetyl-α-D-xylopyranosyl bromide T=20°C; 20 h;
参考文献
Petrovic, Zorica D.; Andjelkovic, Dejan; Spasojevic, Aleksandra
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 1 p. 272 - 275
反应条件
1: n-dodecanol With sodium tetrahydroborate; cyanocobalamin 0.5 h; 2: 2,3,4-tri-O-acetyl-α-D-xylopyranosyl bromide T=20°C; 20 h;
参考文献
Petrovic, Zorica D.; Andjelkovic, Dejan; Spasojevic, Aleksandra
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 1 p. 272 - 275
反应条件
1: butan-1-ol With sodium tetrahydroborate; cyanocobalamin 0.5 h; 2: 2,3,4-tri-O-acetyl-α-D-xylopyranosyl bromide T=20°C; 20 h;
参考文献
Petrovic, Zorica D.; Andjelkovic, Dejan; Spasojevic, Aleksandra
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 1 p. 272 - 275
反应条件
1: 1-nonyl alcohol With sodium tetrahydroborate; cyanocobalamin 0.5 h; 2: 2,3,4-tri-O-acetyl-α-D-xylopyranosyl bromide T=20°C; 20 h;
参考文献
Petrovic, Zorica D.; Andjelkovic, Dejan; Spasojevic, Aleksandra
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 1 p. 272 - 275
反应条件
silver orthophosphate; benzene Behandeln des Reaktionsprodukts mit Chlorwassestoff enthaltendem Methanol;
参考文献
Putman; Hassid
Journal of the American Chemical Society, 1957 , vol. 79, p. 5057,5059
Full Text Show Details
Meagher; Hassid
Journal of the American Chemical Society, 1946 , vol. 68, p. 2135
