2-乙酰氨基-3,4,6-三-O-乙酰-2-脱氧-α-D-吡喃葡萄糖酰基氯合成路线 (共 104 条)
反应条件
aluminum oxide in acetonitrile T=20°C; 2.5 h;
参考文献
Tiwari, Pallavi; Misra, Anup Kumar
Carbohydrate Research, 2006 , vol. 341, # 3 p. 339 - 350
反应条件
hydrogenchloride; acetic anhydride in diethyl ether T=3°C; 72 h;
参考文献
Traar, Pedro; Belaj, Ferdinand; Francesconi, Kevin A.
Australian Journal of Chemistry, 2004 , vol. 57, # 11 p. 1051 - 1053
反应条件
T=4 - 20°C; Inert atmosphere;
参考文献
Orth, Ronald; Pitscheider, Maximilian; Sieber, Stephan A.
Synthesis, 2010 , # 13 art. no. C01710SS, p. 2201 - 2206
参考文献
Macmillan, Derek; Daines, Alison M; Bayrhuber, Monika; Flitsch, Sabine L
Organic letters, 2002 , vol. 4, # 9 p. 1467 - 1470
反应条件
1: 2: With hydrogenchloride T=0 - 25°C;
参考文献
Dolashka-Angelova, Pavlina; Abdel-Jalil, Raid J.; Al-Qawasmeh, Raed A.; Stambolieva, Nicolina; Voelter, Wolfgang
Carbohydrate Research, 2010 , vol. 345, # 16 p. 2343 - 2347
反应条件
hydrogenchloride T=30°C; 16 h; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 71, # 9 p. 3619 - 3622
反应条件
1: 2-amino-2-deoxyglucose hydrochloride With sodium methylate in methanol T=20°C; 2: acetic anhydride T=20°C; 3: With acetyl chloride T=20°C; Further stages.;
参考文献
European Journal of Organic Chemistry, , # 26 p. 4366 - 4375
反应条件
Ambient temperature;
参考文献
Heidlas, Juergen E.; Lees, Watson J.; Pale, Patrick; Whitesides, George M.
Journal of Organic Chemistry, 1992 , vol. 57, # 1 p. 146 - 151
反应条件
1: 2-amino-2-deoxy-D-glucose hydrochloride With sodium methylate in methanol T=20°C; 1 h; 2: acetic anhydride in methanol T=0 - 20°C; 3: With acetyl chloride T=0°C; Inert atmosphereReflux; optical yield given as percent de;
参考文献
Journal of the American Chemical Society, , vol. 132, # 47 p. 16805 - 16811