2-乙酰氨基-3,4,6-三-O-乙酰-2-脱氧-α-D-吡喃葡萄糖酰基氯合成路线 （共 104 条）
反应条件
3 A molecular sieve; mercury(II) iodide in 1,2-dichloro-ethane Ambient temperature;
参考文献
Zemlyakov; Kur'yanov; Chirva
Chemistry of Natural Compounds, 1996 , vol. 32, # 3 p. 352 - 355
反应条件
1: potassium carbonate / acetonitrile / 20 °C 2: cobalt(II) chloride / dichloromethane / 2.5 h / 42 °C View Scheme
参考文献
Kuryanov; Luschtshyk; Chupakhina
Russian Journal of Bioorganic Chemistry, 2013 , vol. 39, # 4 p. 426 - 433
Biokhimiya (Moscow), 2013 , vol. 39, # 4 p. 477 - 485
反应条件
1: 26 percent / Hg(CN)2, HgBr2 2: 6.88 g / NaOMe / methanol / Ambient temperature 3: p-toluenesulphonic acid / acetonitrile / 60 h / 60 °C 4: NaH / tetrahydrofuran View Scheme
参考文献
Lee, Ho Huat; Congson, Ligaya N.; Whitfield, Dennis M.; Radics, Lajos R.; Krepinsky, Jiri J.
Canadian Journal of Chemistry, 1992 , vol. 70, # 10 p. 2607 - 2617
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in dichloromethane 0.75 h; Ambient temperature;
参考文献
Roy, Rene; Tropper, Francois D.
Canadian Journal of Chemistry, 1991 , vol. 69, # 5 p. 817 - 821
反应条件
tin(II) trifluoromethanesulfonate; 4 A molecular sieve; N,N,N',N'-tetramethyl-urea in dichloromethane 48 h; Ambient temperature;
参考文献
Lubineau, Andre; Gallic, Joelle Le; Malleron, Annie
Tetrahedron Letters, 1987 , vol. 28, # 42 p. 5041 - 5044
反应条件
1: 67 percent / tetrabutylammonium hydrogen sulfate, 1M NaOH / CH2Cl2 / 0.75 h / Ambient temperature 2: NaOMe / methanol / Ambient temperature View Scheme
参考文献
Roy, Rene; Tropper, Francois D.
Canadian Journal of Chemistry, 1991 , vol. 69, # 5 p. 817 - 821
反应条件
3 A molecular sieve; mercury(II) iodide in 1,2-dichloro-ethane T=20 - 25°C;
参考文献
Zemlyakov; Kur'yanov; Sidorova; Chirva
Russian Journal of Bioorganic Chemistry, 1998 , vol. 24, # 8 p. 551 - 558
反应条件
3 A molecular sieve; mercury(II) iodide in 1,2-dichloro-ethane T=90 - 95°C;
参考文献
Zemlyakov; Kur'yanov; Sidorova; Chirva
Russian Journal of Bioorganic Chemistry, 1998 , vol. 24, # 8 p. 551 - 558
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in dichloromethane 0.75 h; Ambient temperature;
参考文献
Canadian Journal of Chemistry, , vol. 69, # 5 p. 817 - 821
反应条件
1: 64 percent / Ag2CO3; I2 / CH2Cl2 2: 100 percent / NaOMe; MeOH / 20 °C View Scheme
参考文献
Lee, Ho Huat; Congson, Ligaya N.; Whitfield, Dennis M.; Radics, Lajos R.; Krepinsky, Jiri J.
Canadian Journal of Chemistry, 1992 , vol. 70, # 10 p. 2607 - 2617
