1: in diethyl ether; hexane T=-78 - -60°C; 2 h; 2: With hydrogenchloride in various solvents T=-60 - -40°C; Title compound not separated from byproducts;
参考文献
Abo-Amer, Anwar; Adonin, Nicolay Yu.; Bardin, Vadim V.; Fritzen, Petra; Frohn, Hermann-Josef; Steinberg, Christoph
Journal of Fluorine Chemistry, 2004 , vol. 125, # 11 SPEC. ISS. p. 1771 - 1778
