1-氯-6H-十二氟己烷合成路线 （共 44 条）
16486-97-81-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷
→
反应条件
(NH4)2S2O8; ammonium formate in N,N-dimethyl-formamide T=30 - 40°C;
参考文献
Hu, Chang-Ming; Tu, Ming-Hu
Journal of Fluorine Chemistry, 1991 , vol. 55, # 1 p. 105 - 108
16486-97-81-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷+
→
反应条件
[Co(HDm)2Py]Br; zinc in ethanol T=30°C; 2 h;
参考文献
Hu, Chan-Ming; Qiu, Yao-Ling
Journal of Organic Chemistry, 1992 , vol. 57, # 12 p. 3339 - 3342
16486-97-81-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷+
→
反应条件
[Co(HDm)2Py]Br; zinc in ethanol T=20°C; 1 h;
参考文献
Hu, Chan-Ming; Qiu, Yao-Ling
Journal of Organic Chemistry, 1992 , vol. 57, # 12 p. 3339 - 3342
16486-97-81-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷+
→
反应条件
[Co(HDm)2Py]Br; zinc in ethanol T=15°C; 0.5 h;
参考文献
Hu, Chan-Ming; Qiu, Yao-Ling
Journal of Organic Chemistry, 1992 , vol. 57, # 12 p. 3339 - 3342
16486-97-81-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷
→
反应条件
[Co(HDm)2Py]Br; zinc in ethanol T=25°C; 2 h;
参考文献
Hu, Chan-Ming; Qiu, Yao-Ling
Journal of Organic Chemistry, 1992 , vol. 57, # 12 p. 3339 - 3342
16486-97-81-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷+
→
反应条件
[Co(HDm)2Py]Br; zinc in ethanol T=30°C; 5 h;
参考文献
Hu, Chan-Ming; Qiu, Yao-Ling
Journal of Organic Chemistry, 1992 , vol. 57, # 12 p. 3339 - 3342
16486-97-81-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷
→
反应条件
sodium; ethyl acetoacetate in ethanol; N,N-dimethyl-formamide T=75°C; 10 h;
参考文献
CHEN,Q.Y.; QUI,Z.M.
Journal of Fluorine Chemistry, 1987 , vol. 35, p. 343
16486-97-81-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷
→
反应条件
magnesium in tetrahydrofuran 5 h; Heating;
参考文献
Chen, Quing-Yun; Qiu, Zai-Ming; Yang, Zhen-Yu
Journal of Fluorine Chemistry, 1987 , vol. 36, p. 149 - 162
16486-97-81-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷
→
反应条件
tetrakis(triphenylphosphine) palladium(0) in hexane T=60°C; 0.5 h;
参考文献
Huang, Yao-Zeng; Shou, Qi-Lin
Journal of Organic Chemistry, 1987 , vol. 52, # 16 p. 3552 - 3558
16486-97-81-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷
→
反应条件
tetrakis(triphenylphosphine) palladium(0) in hexane T=60°C; 0.5 h;
参考文献
Huang, Yao-Zeng; Shou, Qi-Lin
Journal of Organic Chemistry, 1987 , vol. 52, # 16 p. 3552 - 3558
